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Organic Syntheses Without Solvent: Preparation of Alkoxyphthalimides and of Alkoxylamines |
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| Authors: | Herve Galons Jean Fiet Claude Combet-farnoux Marcel Miocque Georges Bram |
| Affiliation: | 1. UA 496 du CNRS, Faculté de Pharmacie , Rue J.B. Clément , F-92296 Chǎtenay-Malabry, France;2. UA 478 du CNRS, Bǎtiment 410 , Université Paris Sud , F-91405, Orsay, France;3. UA 496 du CNRS, Faculté de Pharmacie , Rue J.B. Clément , F-92296 Chǎtenay-Malabry, France |
| Abstract: | Alkoxyphthalimides are prepared by alkylation of N-hydroxyphthalimide under solid-liquid phase transfer catalysis without solvent. When conversion of alkoxyphthalimides into alkoxylamines is nearly complete, neat hydrazine hydrate is added at room temperature. |
| Keywords: | Manganese(II) complexes nitroxide free radicals |