Pyrazolines — Derivatives of 2-nitrochalcone |
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Authors: | V. D. Orlov N. V. Getmanskii O. V. Shishkin E. E. Lakin V. P. Kuznetsov |
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Affiliation: | (1) Kharkov State University, 310077 Kharkov;(2) Institute for Single Crystals, Ukrainian Academy of Sciences, 310141 Kharkov |
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Abstract: | By the reaction of 2-nitrochalcone with hydrazine hydrate, 5-(2-nitrophenyl)-3-phenyl-1H-2-pyrazoline (I) and the hydrazone of 3-(5-(2-nitrophenyl)-3-phenyl-2-pyrazolin-1-yl)-3-(2-nitrophenyl)propiophenol (II) have been prepared. The acylation of both compounds I and II leads to N-acyl derivatives of the first. The acylating ability of formamide and N,N-dimethylformamide was observed in reactions with pyrazoline I. An x-ray structural study was carried out on compound II.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 3, pp. 360–366, March, 1993. |
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