| 气相色谱质谱法分析土壤中多溴联苯和多溴联苯醚类化合物 |
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| 引用本文： | 余彬彬,方铖,饶钦全,陈涛,牟义军,吴祖成.气相色谱质谱法分析土壤中多溴联苯和多溴联苯醚类化合物[J].分析化学,2011,39(6):833-838. |
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| 作者姓名： | 余彬彬 方铖 饶钦全 陈涛 牟义军 吴祖成 |
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| 作者单位： | 余彬彬,YU Bin-Bin(浙江大学环境科学研究所能源清洁利用国家重点实验室,杭州,310027;台州市环境监测中心站,台州,318000);方铖,饶钦全,陈涛,牟义军,FANG Cheng,RAO Qin-Quan,CHEN Tao,MOU Yi-Jun(台州市环境监测中心站,台州,318000);吴祖成,WU Zu-Cheng(浙江大学环境科学研究所能源清洁利用国家重点实验室,杭州,310027) |
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| 摘 要： | 建立了气相色谱-质谱法(GC-MS)分析土壤中的18种多溴联苯(PBBs)和多溴联苯醚类(PBDEs)化合物的方法.利用快速溶剂萃取(ASE)技术和凝胶净化系统(GPC)进行土壤样品的前处理,(13)C标记物作为进样内标和替代标,采用电子轰击源气相色谱质谱法(GC-EI/MS )分析-溴至七溴代PBBs和PBDEs,负...
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| 关 键 词： | 多溴联苯醚 多溴联苯 气相色谱质谱法 土壤 |
Determination of Polybrominated Diphenyl Ethers and Polybromominated Biphenyls in Soil by Gas Chromatography-Mass Spectrometry |
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| YU Bin-Bin,FANG Cheng,RAO Qin-Quan,CHEN Tao,MOU Yi-Jun,WU Zu-Cheng.Determination of Polybrominated Diphenyl Ethers and Polybromominated Biphenyls in Soil by Gas Chromatography-Mass Spectrometry[J].Chinese Journal of Analytical Chemistry,2011,39(6):833-838. |
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| Authors: | YU Bin-Bin FANG Cheng RAO Qin-Quan CHEN Tao MOU Yi-Jun WU Zu-Cheng |
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| Institution: | YU Bin-Bin1,2,FANG Cheng2,RAO Qin-Quan2,CHEN Tao2,MOU Yi-Jun2,WU Zu-Cheng*1 1(Department of Environmental Engineering,State Key Laboratory of Clean Energy Utilization,Zhejiang University,Hangzhou 310027) 2(Environmental Monitoring Center of Taizhou,Taizhou 318000) |
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| Abstract: | A gas chromatography-mass spectrometry(GC-MS) was used for the determination of 18 kinds of polybrominated diphenyl ethers(PBDEs) and polybromominated biphenyls(PBBs) in soils.The sample was extracted by accelerated solvent extraction(ASE) and cleaned up by gel permeation chromatographic technique(GPC).13C-labeled PCB and PBDE were added as internal standard and surrogate compound for quantitative determination.GC-EI/MS was used to analyze low-brominated PBDEs and PBBs,while GC-NCI/MS was applied for high-b... |
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| Keywords: | Polybrominated diphenyl ethers(PBDEs) Polybromominated biphenyl(PBBs) Gas chromatography mass spectrometry(GC-MS) Soil |
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