| 1,5-二芳基-3-氯甲基硫代-1H-1,2,4-三唑的合成及其结构表征 |
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| 引用本文： | 刘天宝,彭艳芬,伍光辉,汪新.1,5-二芳基-3-氯甲基硫代-1H-1,2,4-三唑的合成及其结构表征[J].光谱实验室,2011,28(4):1859-1861. |
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| 作者姓名： | 刘天宝 彭艳芬 伍光辉 汪新 |
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| 作者单位： | 池州学院化学材料与工程实验中心 安徽省池州市建设西路168号247000 |
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| 基金项目： | 安徽省自然科学基金资助项目，安徽省教育厅自然科学基金资助项目，安徽省高等学校省级优秀青年人才基金资助项目 |
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| 摘 要： | 1-芳酰基-3-苯氨基硫脲与二氯甲烷在无溶剂条件下反应合成了4种1,5-二芳基-3-氯甲基硫代-1H-1,2,4-三唑类化合物,产率为64%-74%.产物的结构通过红外光谱、核磁共振光谱和高分辨质谱进行了表征.
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| 关 键 词： | 三唑 1-芳酰基-3-苯氨基硫脲 二氯甲烷 |
Synthesis and Characterization of 1,5-Diaryl-3-Chloromethylthio-1H-1,2,4-Triazole |
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| LIU Tian-Bao,PENG Yan-Fen,WU Guang-Hui,WANG Xin.Synthesis and Characterization of 1,5-Diaryl-3-Chloromethylthio-1H-1,2,4-Triazole[J].Chinese Journal of Spectroscopy Laboratory,2011,28(4):1859-1861. |
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| Authors: | LIU Tian-Bao PENG Yan-Fen WU Guang-Hui WANG Xin |
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| Institution: | LIU Tian-Bao PENG Yan-Fen WU Guang-Hui WANG Xin(Center of Chemical Engineering and Materials Science,Chizhou University,Chizhou,Anhui 247000,P.R.China) |
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| Abstract: | Four kinds of 1,5-diaryl-3-chloromethylthio-1H-1,2,4-triazole compounds were prepared by the reaction of 1-aroyl-3-phenylaminothiourea with dichloromethane.All the structures of compounds were confirmed by IR,1H NMR,13C NMR and HRMS spectra.The yields were about 64%—74%. |
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| Keywords: | Triazole 1-Aroyl-3-Phenylaminothiourea Dichloromethane |
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