The reaction of hexamethyl phosphoric triamide (HMPT) with phosphoryl chloride : A reexamination. Application to a novel preparation of BOP reagent for peptide coupling |
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Authors: | Jean-Robert Dormoy Bertrand Castro |
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Institution: | Laboratoire de Chimie Organique II, Université de Nancy I Case Officielle 140, 54037 Nancy France |
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Abstract: | The reaction of hexamethyl phosphoric triamide with phosphoryl chloride at R.T. gave actually a chlorophosphonium salt. This reaction is illustrated in a novel preparation of BOP reagent for peptide coupling in good conditions. |
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