| ICP-AES法测定粗氧锑中砷硒 |
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| 引用本文： | 马晓国,梁奕昌,成晓玲,吴惠玲,谭锟嵛.ICP-AES法测定粗氧锑中砷硒[J].理化检验(化学分册),2000,36(1):18-19. |
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| 作者姓名： | 马晓国 梁奕昌 成晓玲 吴惠玲 谭锟嵛 |
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| 作者单位： | 广东工业大学分析测试中心,广州,510090 |
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| 摘 要： | ３用浓硫酸溶解粗氧锑，ＩＣＰ－ＡＥＳ法直接测定砷。对于样品中的痕量硒，先以次磷酸钠还原单质，并与砷共沉淀，经浮选分离后再测定。对硒的分离条件进行了优化。考察了基体锑的干扰及共存杂质的影响。方法运用于粗氧锑样品中砷、硒测定、结果满意。
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| 关 键 词： | ICP－AES 粗氧锑 砷 硒 浮选分离 |
| 修稿时间： | 1999-06-07 |
ICP-AES DETERMINATION OF ARSENIC AND SELENIUM IN ANTIMONY TRIOXIDE |
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| Ma Xiaoguo,Liang Yichang,Cheng Xianling,Wu Hailing,Tan Kunya.ICP-AES DETERMINATION OF ARSENIC AND SELENIUM IN ANTIMONY TRIOXIDE[J].Physical Testing and Chemical Analysis Part B:Chemical Analgsis,2000,36(1):18-19. |
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| Authors: | Ma Xiaoguo Liang Yichang Cheng Xianling Wu Hailing Tan Kunya |
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| Institution: | Ma Xiaoguo
,Liang Yichang
,Cheng Xianling
,Wu Hailing
,Tan Kunya
;(Analytical Center, Guangdong University of Technology Guangzhou 510090) |
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| Abstract: | It is reported in this paper that arsenic in antimony trioxide can be determined by ICP-AES directly in the sample dissolved in conc sulfuric acid. The selenium in the sample is determined after a floatation separation. |
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| Keywords: | ICP-AES determination Antimony trioxide Arsenic Selenium Floatation separation |
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