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| 几种新型呋喃胺Schiff碱的合成 | |
| 引用本文： | 李艳,胡杨根,丁明武.几种新型呋喃胺Schiff碱的合成[J].武汉大学学报(理学版),2011,57(1). |
| 作者姓名： | 李艳 胡杨根 丁明武 |
| 作者单位： | 1. 咸宁学院,化学与生命科学学院,湖北,咸宁,437100 2. 郧阳医学院,医学化学研究所,湖北,十堰,442000 3. 华中师范大学,农药与化学生物学教育部重点实验室,湖北,武汉,430079 |
| 基金项目： | 国家自然科学基金(20772041)资助项目 |
| 摘 要： | 以自制的5-甲基-4-乙氧羰基-3-腈基-2-呋喃胺与取代芳醛为主要原料,以乙醇为溶剂、醋酸为催化剂,通过回流反应以70%～85%的产率合成了8种新的5-甲基-4-乙氧羰基-3-腈基-2-呋喃胺Schiff碱化合物,产物用紫外-可见吸收光谱,红外光谱,核磁共振氢谱和质谱进行了表征. |
| 关 键 词： | 呋喃胺 Schiff碱 合成 |
Synthesis of Some New Kinds of Furan Amine Schiff Bases |
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| LI Yan,HU Yanggen,DING Mingwu.Synthesis of Some New Kinds of Furan Amine Schiff Bases[J].JOurnal of Wuhan University:Natural Science Edition,2011,57(1). | |
| Authors: | LI Yan HU Yanggen DING Mingwu |
| Institution: | LI Yan1,HU Yanggen2,DING Mingwu3(1.College of Chemistry and Life Science,Xianning College,Xianning 437100,Hubei,China,2.Institute of Medicinal Chemistry,Yunyang Medical College,Shiyan 442000,3.Key Laboratory of Pesticide and Chemical Biology of Ministry of Education,Huazhong Normal University,Wuhan 430079,China) |
| Abstract: | Eight new 3-cyano-4-ethoxycarbonyl-5-methyl-2-furan amine Schiff bases were synthesized from self-made 3-cyano-4-ethoxycarbonyl-5-methyl-2-furan amine and aromatic aldehydes using alcohol as dissolvent,acetic acid as the catalyst by reflux in yield of 70%-85%.Their structures were confirmed by UV-vis,IR,1H NMR and MS. |
| Keywords: | furan amine Schiff base synthesis |
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