| 偏振-同步荧光法同时测定(艹屈)、蒽和苝 |
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| 引用本文： | 顾丽忠,黄承玲,翁毅滨,黄贤智,陈国珍.偏振-同步荧光法同时测定(艹屈)、蒽和苝[J].光谱学与光谱分析,1993(3). |
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| 作者姓名： | 顾丽忠 黄承玲 翁毅滨 黄贤智 陈国珍 |
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| 作者单位： | 淅江工学院化工系，厦门大学化学系，厦门大学化学系，厦门大学化学系，厦门大学化学系 310014 杭州，361005 厦门，361005 厦门，361005 厦门，361005 厦门 |
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| 摘 要： | 在荧光分光光度计的激发和发射光路中分别置入偏振互为垂直的偏振片,能有效地抑制同步扫描过程中散射光的影响。建立了(艹屈)蒽和苝的同时偏振-同步荧光分析法,其检出限改善3.9倍,相对标准偏差小于3.1%。
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| 关 键 词： | 偏振 同步荧光法 (艹屈) 蒽 苝 |
SIMULTANEOUS DETERMINATION OF TRACE CHRYSENE ANTHRACENE AND PERYLENE BY POLARIZATION SYNCHRONOUS SPECTROFLUORIMETRY |
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| GU Lizhong Zhejiang Institute of Technology, Hangzhou HUANG Changlin WONG Yibin HUANG Xianzhi CHEN Guozhen Xiamen University, Xiamen.SIMULTANEOUS DETERMINATION OF TRACE CHRYSENE ANTHRACENE AND PERYLENE BY POLARIZATION SYNCHRONOUS SPECTROFLUORIMETRY[J].Spectroscopy and Spectral Analysis,1993(3). |
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| Authors: | GU Lizhong Zhejiang Institute of Technology Hangzhou HUANG Changlin WONG Yibin HUANG Xianzhi CHEN Guozhen Xiamen University Xiamen |
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| Institution: | GU Lizhong Zhejiang Institute of Technology,310014 Hangzhou HUANG Changlin WONG Yibin HUANG Xianzhi CHEN Guozhen Xiamen University,361005 Xiamen |
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| Abstract: | This work is performed on a spectrofluorimeter, which is equipped with two vertical polarizers in both the excitation and the emission light paths. The use of this technique can effectively suppress the effect of scattered light during synchronous scanning. A new method of polarization synchronous spectrofluorimetry for the simultaneous determination of chrysene, anthracene and perylene is described. The detection limit is nearly a fourfold decrease. The relative standard deviation is less than 3.1%. |
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| Keywords: | Chrysene Anthracene Perylene Polarization Synchronous spectrofluorimetry |
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