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| ICP-AES测定硅锰中的磷 | |
| 引用本文： | 黄梅,方智,何会珍,王锡丽. ICP-AES测定硅锰中的磷[J]. 分析试验室, 2011, 30(9): 96-99 |
| 作者姓名： | 黄梅 方智 何会珍 王锡丽 |
| 作者单位： | 1. 成都农业科技职业学院,成都,611130 2. 四川出入境检验检疫局,成都,610041 |
| 摘 要： | 采用电感耦合等离子体-原子发射光谱法(ICP-AES)研究了硅锰合金中磷的测定,考察了试样的分解、分析谱线的选择、干扰元素的影响及精密度和准确度等影响的有关因素,其测定结果与国家标准方法一致.磷的分析谱线采用214.914 nm的测定结果最好；该方法的检出限为0.003％,回收率为96.9％～101.6 ％. |
| 关 键 词： | 硅锰合金 磷 电感耦合等离子体-原子发射光谱法 |
Determination of phosphorus in ferromanganese-silicon by ICP-AES |
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| HUANG Mei,FANG Zhi,HE Hui-zhen,WANG Xi-li. Determination of phosphorus in ferromanganese-silicon by ICP-AES[J]. Chinese Journal of Analysis Laboratory, 2011, 30(9): 96-99 | |
| Authors: | HUANG Mei FANG Zhi HE Hui-zhen WANG Xi-li |
| Affiliation: | HUANG Mei 1,FANG Zhi2,HE Hui-zhen2 and WANG Xi-li2(1.Chengdu Vocational College of Agricultural Science and Technology,Chengdu 611130,2,Sichuan Entry-Exit Inspection and Quarantine Burare of the People,s Republic of China,Chengdu 610041),Fenxi Shiyanshi,2011,30(9):96~99 |
| Abstract: | The determination of phosphorus in ferromanganese-silicon was investigated by inductively coupled plasma atomic emission spectrometry(ICP-AES),and the effect of various factors on the testing results,the conditions of dissolving the sample,selection of spectral lines,interference elements,as well as the accuracy and the precision,were discussed in the paper.The experimental results are in accordance with those by the national standard and the method has been approved by China NIL Research Center for Profici... |
| Keywords: | Ferromanganese-silicon Phosphorus Inductively Coupled Plasma Atomic Emission Spectrometry |
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