| 新的双枝[1,3,4]-噁二唑衍生物的设计与微波合成 |
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| 引用本文： | 梅青刚,吴双,赵志刚.新的双枝[1,3,4]-噁二唑衍生物的设计与微波合成[J].化学研究与应用,2011,23(5):521-527. |
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| 作者姓名： | 梅青刚 吴双 赵志刚 |
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| 作者单位： | 1. 西南民族大学化学与环境保护工程学院,四川,成都,610041
2. 西南民族大学电气信息工程学院,四川,成都,610041 |
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| 基金项目： | 国家外专局外国专家资助项目(2009-15) |
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| 摘 要： | 在微波辐射条件下,以三氯氧磷作环合剂,以双酰肼为中间体,快速有效地合成了一系列新的1,3-二(5-芳基-1,3,4-噁二唑-2-基)甲氧基]苯类化合物.十二个目标化合物(5a-5l)和五个中间体(4c,4d,4e,4j,4k)均为未见文献报道的新化合物,其结构经核磁、红外、质谱和元素分析所确证.该方法的显著优点是简单...
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| 关 键 词： | 酰肼 双枝噁二唑衍生物 微波辐射 |
Design and synthesis of bis-1,3,4-oxadiazole derivatives under microwave irradiation |
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| MEI Qing-gang,WU Shuang,ZHAO Zhi-gang.Design and synthesis of bis-1,3,4-oxadiazole derivatives under microwave irradiation[J].Chemical Research and Application,2011,23(5):521-527. |
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| Authors: | MEI Qing-gang WU Shuang ZHAO Zhi-gang |
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| Institution: | MEI Qing-gang1,WU Shuang2,ZHAO Zhi-gang 1 (1.College of Chemistry and Environmental Protection Engineering,Southwest University for Nationalities,Chengdu,610041,China,2.College of Electric and Information Engineering,Chengdu 610041,China) |
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| Abstract: | A series of novel bis-1,3,4-oxadiazole derivatives were synthesized under microwave irradiation with the cyclization of various dicarboxylic dihydrazides.Twelve target compounds and five intermediates were new compounds and their structures were characterized by 1H NMR,IR,MS spectra and elemental analysis.The distinct advantages of this method were simple,rapid and efficient. |
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| Keywords: | dihydrazides bis-1 3 4-oxadiazole derivatives microwave irradiation |
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