Abstract: | Abstract The quantitative determination of formaldehyde in air using the fluorimetric acetylacetone method is described. Known concentrations of formaldehyde were generated and collected in water using abosorbers. The sampling rate was 0.5 1/min, and the sampling volumes varied from 2 to 20 1, depending on the concentration level. Under these conditions the entire sampling and the analytical method were evaluated over a range of 0.2–1.7 mg formaldehyde per m3 of air. The precision of the method expressed as a mean value of the relative standard deviation of 7 independent measurements (6 single determinations each) was (3.4 ± 1.6) % (SD). The accuracy was (101 ± 5) % (SD). The detection limit of the method was estimated to be 0.040 mg formaldehyde per m3 of air (5 liter air sample). |