Determination of water in thiols by Karl Fischer titration |
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Authors: | Francis H J Persing D D |
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Affiliation: | Pennwalt Corporation, 900 First Avenue, P.O. Box C, King of Prussia, Pennsylvania 19406, U.S.A. |
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Abstract: | Water in thiol-containing samples may be determined by titration with Karl Fischer reagent after conversion of the thiol into a thioether. Both acrylonitrile and N-ethylmaleimide have been found to be suitable reagents. |
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