One-pot Preparation of Fluorinated Polyhydrobenzoacridine-1-one Derivatives under Microwave Irradiation and Solvent-free Conditions |
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| Authors: | Jin Jianan Zhang Jianmin Liu Fengrui Shang Wenli Xin Yong Zhu Shizheng |
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| Affiliation: | 1. Department of Chemistry, School of Science, Shanghai University, Shanghai 200444, China;2. Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China |
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| Abstract: | A facile and efficient synthesis of fluorine‐containing polyhydrobenzoacridines was accomplished by a three‐component coupling of fluorinated aldehyde, α‐naphthylamine, and 1,3‐cyclohexanedione or dimedone under microwave irradiation and solvent‐free conditions without catalyst. All new compounds were obtained in moderate to good yields and characterized by standard spectroscopic methods. |
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| Keywords: | fluorinated polyhydrobenzoacridines condensation reaction microwave irradiation one‐pot three‐component coupling |
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