| CRYSTAL AND MOLECULAR STRUCTURE OF (μ-PhS) (μ-σ,π-CH_3CH = CH)Fe_2(CO)_6 |
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| 引用本文： | 宋礼成,周忠远,等.CRYSTAL AND MOLECULAR STRUCTURE OF (μ-PhS) (μ-σ,π-CH_3CH = CH)Fe_2(CO)_6[J].结构化学,1990,9(1):34-37. |
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| 作者姓名： | 宋礼成 周忠远 等 |
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| 基金项目： | Project supported by the National Science Foundation of China |
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| 摘 要： | <正> The crystal and molecular structure of (μ-PhS) (μ-σ, n-CH3CH = CH)-Fe2(CO)6 has been determined by X - ray diffraction technique. The complex has chemical formula of C15H10O6SFe2 and Mr=129. 99. The crystals are monoclinic,space group P21/c,with α=11. 789(2),b= 7. 159(1),c = 20. 890(4) A ;β = 100. 89(2);V = 1731. 32 A3;Z=4,Dc=1. 65g·cm-3;F(000) = 863. 86. The final R and Rw equal 0. 0315 and 0. 0405 respectively for 2527 observed unique reflections.
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| 关 键 词： | 晶体结构 分子结构 苯硫酚 铁配合物 丙烯 链烯基 |
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