Structural and spectral study of 7-bromo-1,3-dihydro-5-(2-pyridyl)-2H-1,4-benzodiazepin-2-one (bromazepam) platinum(II) dichloride bisdimethylsulfoxide |
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Authors: | Adriano Benedetti Antonio C. Fabretti Carlo Preti Giuseppe Tosi Paolo Zannini |
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Affiliation: | (1) Centro Interdipartimentale Grandi Strumenti, University of Modena, Via G. Campi, 213, 41100 Modena, Italy;(2) Dipartimento di Chimica, University of Modena, Via G. Campi, 183, 41100 Modena, Italy |
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Abstract: | The synthesis and crystal and molecular structure of the title compound are reported. It belongs to the monoclinic space groupC2/c, witha=17.889(2),b=13.511(1),c=19.912(2) Å,=99.841(4)°, andZ=8. The structure was refined to a finalR of 2.77% (Rw=2.88%) for 3617 observed reflections. Vibrational spectra are recorded and discussed. |
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