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Preparation and condensation reactions of a new light-fluorous Mukaiyama reagent: reliable purification with fluorous solid phase extraction for esters and amides |
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| Authors: | Masato Matsugi Masakazu Hasegawa Sachina Okamoto Yoshimi Ikeya Yuji Mori |
| Institution: | a Faculty of Agriculture, Meijo University, 1-501 Shiogamaguchi, Tempaku, Nagoya 468-8502, Japan b Faculty of Engineering, Osaka Institute of Technology, 5-16-1 Omiya, Asahi, Osaka 535-8585, Japan c Faculty of Pharmacy, Meijo University, 150, Yagotoyama, Tempaku, Nagoya 464-8606, Japan |
| Abstract: | A modified light-fluorous Mukaiyama reagent bearing a C8F17 tag was prepared and examined in ester and amide forming condensation reactions. Following the reactions, the desired product was effectively separated from the fluorous pyridone by-product using a simple fluorous solid phase extraction. |
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