| [Mn(H_2O)_4(NCS)_2)(18C6)和(Co(H_2O)_4(NCS)_2)(18C6)单晶的培养及物性表征 |
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| 引用本文： | 杜高英,张文兴,樊悦朋.[Mn(H_2O)_4(NCS)_2)(18C6)和(Co(H_2O)_4(NCS)_2)(18C6)单晶的培养及物性表征[J].高等学校化学学报,1988(8). |
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| 作者姓名： | 杜高英 张文兴 樊悦朋 |
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| 作者单位： | 山东省分析测试中心
(杜高英)，山东大学化学系
(张文兴)，山东大学化学系(樊悦朋) |
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| 摘 要： | 用凝胶法和蒸发法分别培养出配合物Mn(H_2O)_4(NCS)_2]18C6)和Co(H_2O)_4(NCS)_2](18C6)的单晶。对两个配合物进行了溶解性能的测试、元素分析、电导测量、红外光谱分析、热分析和质谱分析。表征的指派为晶体结构分析结果所证实。 。。
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| 关 键 词： | 冠醚配合物 单晶的培养 冠醚性质 |
The Crystal Crowth and Their Properties of cMn(H_2O)_4(NCS)2](18C_6) and cCo(H_2O)_4(NCS)_2](18C_6) |
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| Du Gaoying.The Crystal Crowth and Their Properties of cMn(H_2O)_4(NCS)2](18C_6) and cCo(H_2O)_4(NCS)_2](18C_6)[J].Chemical Research In Chinese Universities,1988(8). |
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| Authors: | Du Gaoying |
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| Abstract: | The crystal growth of CMn(H2O)4(NCS)2](18C6) and Co(H2O)4-(NCS)2](18,C6) were separated by gel diffusion method and solvent evaporation method.The pink slice like crystal and rose red lump like crystal were obtaimed. The elememtal analyses of complex crystals was done.The properties of solubility, electroconductivity measurement, IR, DTA-TG-DTG analyses. and MS were respectively tested. All results above and their designation were confirmed by X-ray single crystal structure analysis. |
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| Keywords: | Crown complexes Single crystal goovvth Crown properties |
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