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A facile cyclopropanol synthesis from β-halo ester with grignard reagent-samarium(II) diiodide couple |
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| Authors: | Shin-ichi Fukuzawa Yasuhiko Niimoto Shizuyoshi Sakai |
| Institution: | Department of Applied Chemistry, Faculty of Science and Engineering, Chuo University, Kasuga, Bunkyo-ku, Tokyo 112, Japan a Department of Materials Science, Faculty of Engineering, Shizuoka University, Hamamatsu, Shizuoka 432, Japan |
| Abstract: | Transformation of  ,β-halo ester to the cyclopropanols by a coupled reagent of samarium(II) diiodide with Grignard reagent in tetrahydrofuran-hexamethylphosphoric triamide was very successfully under mild conditions. |
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