Synthesis and Crystal Structure of Mixed-Ligand Ni(II) Complex of N-(1-Phenyl-3-methyl-4-benzylidene-5-pyrazolone) p-Nitrobezoylhydrazide and Pyridine |
| |
| Authors: | Zhang Li Liu Lang Jia Dianzeng Yu Kaibei |
| |
| Institution: | (1) Institute of Applied Chemistry, Xinjiang University, Urumqi, 830046, People's Republic of China;(2) Chengdu Institute of Organic Chemistry, Chinese Academy of Sciences, Chengdu, 610012, People's Republic of China |
| |
| Abstract: | A novel mixed-ligand nickel complex, Ni(PMBP—PNH) (Py)3], PMBP—PNH=N-(1-phenyl-3-methyl-4-benzylidene-5-pyrazolone) p-nitrobezoylhydrazide; Py = pyridine], has been synthesized by the hydrothermal method and characterized by elemental analysis, IR spectrum, thermal analysis, and single-crystal X-ray diffraction. The X-ray diffraction reveals that the nickel (II) ion in the title complex is in a slightly distorted octahedral arrangement of the ONO donor atoms of primary ligand PMBP-PNH and three N-donor atoms in the secondary ligand pyridine. |
| |
| Keywords: | Crystal structure hydrothermal synthesis mixed-ligand complex nickel (II) complex |
| 本文献已被 SpringerLink 等数据库收录！ |
|
