Regioselective synthesis and structural elucidation of 1,4-disubstituted 1,2,3-triazole derivatives using 1D and 2D NMR spectral techniques |
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| Authors: | Babu Thelagathoti Hari Kumar B V N Phani Rajeswari C Perumal Paramasivan T |
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| Institution: | 1. Organic Chemistry Division, Central Leather Research Institute, , Adyar, Chennai, 600 020 India;2. Chemical Physics Laboratory, Central Leather Research Institute, , Adyar, Chennai, 600 020 India |
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| Abstract: | Regioselective synthesis of 2-1-(2-oxo-2-phenylethyl)-1H-1,2,3]triazol-4-ylmethoxy]-benzaldehyde derivatives was achieved by 3 + 2] cycloaddition reaction of 2-(prop)-2-ynyloxy-benzaldehyde derivatives with phenacyl azide. The regiochemistry and the spectral assignments of the synthesized triazole derivatives were studied using both 1D and 2D NMR spectral techniques in solution. |
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| Keywords: | 1H NMR 13C NMR 2D NMR 1 4‐disubstituted 1 2 3‐triazoles |
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