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Synthesis and solid-state structures of new cyclophane host molecules |
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| Authors: | Bronislaw P. Czech Christopher M. Stetson Richard A. Bartsch |
| Affiliation: | a Department of Chemistry and Biochemistry, Texas Tech University, Lubbock, TX 79409, USA b Department of Chemistry, Silesian University, 9 Szkolna Street, 40-006 Katowice, Poland c Department of Chemistry and Biochemistry, Brigham Young University, Provo, UT 84602, USA |
| Abstract: | Five new cyclophane host molecules (corrals) are prepared by linking together two α,α′-di(4-hydroxyphenyl)-1,4-diisopropylbenzene or α,α′-di(3,5-dimethyl-4-hydroxyphenyl)-1,4-diisopropylbenzene units with two permethylene spacers. Three small cyclophane hosts (boxes) are synthesized by cyclization of α,α′-di(4-hydroxyphenyl)-1,4-diisopropylbenzene with di(bromomethyl)benzene compounds. Solid-state structures of one corral and one box are reported. |
| Keywords: | Cyclophane synthesis Solid-state structures |
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