|
|||||
|
|
| 超声波提取-固相萃取净化-气相色谱法分析烟草中拟除虫菊酯类农药及氟节胺残留 | |
| 引用本文： | 石杰,杨静,刘惠民,胡斌,吴家锴,严会会. 超声波提取-固相萃取净化-气相色谱法分析烟草中拟除虫菊酯类农药及氟节胺残留[J]. 分析试验室, 2010, 29(4) |
| 作者姓名： | 石杰 杨静 刘惠民 胡斌 吴家锴 严会会 |
| 作者单位： | 郑州大学化学系,郑州,450052;中国烟草总公司郑州烟草研究院,郑州,450001 |
| 基金项目： | 河南省科技攻关(0496430006);;河南省自然科学基础研究(0411021200)项目资助 |
| 摘 要： | 建立了超声波提取-固相萃取净化-气相色谱联用测定烟草中多种拟除虫菊酯类农药及氟节胺残留量的方法。与现行标准方法相比,本方法前处理简单、快速、有机溶剂消耗量少,且增加了分析目标物的数量。8种拟除虫菊酯类农药及氟节胺在0.1、0.5和1μg/g三个加标水平的回收率为86%～111%,相对标准偏差为0.2%～4.1%,满足当前烟草农药残留的检测要求。 |
| 关 键 词： | 拟除虫菊酯类农药 氟节胺 超声波提取 烟草 |
Study on determination of pyrethroid and flumetralin pesticide residues in tobacco by gas chromatography combined with ultrasonic extraction and solid phase extraction |
|
| SHI Jie,YANG Jing,LIU Hui-min,HU Bin,WU Jia-kai,YAN Hui-hui. Study on determination of pyrethroid and flumetralin pesticide residues in tobacco by gas chromatography combined with ultrasonic extraction and solid phase extraction[J]. Chinese Journal of Analysis Laboratory, 2010, 29(4) | |
| Authors: | SHI Jie YANG Jing LIU Hui-min HU Bin WU Jia-kai YAN Hui-hui |
| Affiliation: | 1.Department of Chemistry;Zhengzhou University;Zhengzhou 450052;2.Zhengzhou Tobacco Research Institute of CNTC;Zhengzhou 450001 |
| Abstract: | A method for the determination of pyrethroid and flumetralin pesticide residues in tobacco had been developed.Samples were extracted by ultrasonic and cleaned up on a Florisil solid phase extraction column.Eight pyrethroid and flumetralin quantification were achieved by gas chromatography with an electron capture detector (GC-ECD).Compared with the available standard method of GB/T 13595-2004,the pretreatment of the new method was easy,rapid,cheap and less solvent consumption.The recoveries of eight pyrethr... |
| Keywords: | Pyrethroids pesticides Flumetralin Ultrasonic extraction Tobacco |
| 本文献已被 CNKI 万方数据 等数据库收录！ | |