| 电感耦合等离子体原子发射光谱(ICP-AES)法测定蒙药巴特日中17种元素的含量 |
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| 引用本文： | 宝力道,乌兰其其格,赵玉英.电感耦合等离子体原子发射光谱(ICP-AES)法测定蒙药巴特日中17种元素的含量[J].中国无机分析化学,2016,6(4):1-3. |
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| 作者姓名： | 宝力道 乌兰其其格 赵玉英 |
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| 作者单位： | 1. 赤峰学院口腔医学院,内蒙古赤峰,024000;2. 内蒙古民族大学分析测试中心,内蒙古通辽,028043 |
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| 基金项目： | 内蒙古自然基金(2015MS0221)；通辽市与内蒙古民族大学科技合作项目(SXYB2012032)；内蒙古卫生厅项目(201302150)资助 |
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| 摘 要： | 建立了快速、准确同时测定蒙药巴特日中多种元素含量的方法。采用电感耦合等离子体原子发射光谱(ICP-AES)法同时测定了蒙药巴特中17种常量、微量及重金属元素的含量,进行了加标回收实验,结果表明,巴特日中Ca、P、K的含量较高,富含Fe和Mg等营养元素,Pb、Cd等重金属元素均低于国家标准。相对标准偏差(RSD)在0.36%~0.86%,加标回收率为95.8%~103%。测定的实验数据准确,可靠,可用于蒙药巴特日中多种元素的同时测定。
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| 关 键 词： | 蒙药巴特日 ICP-AES 多元素 同时测定 |
| 收稿时间： | 2016/4/12 0:00:00 |
| 修稿时间： | 2016/5/20 0:00:00 |
Determination of Seventeen Elements in Mongolian Medicine Bateri by ICP-AES |
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| BAO Lidao,WU Lanqiqige and ZHAO Yuying.Determination of Seventeen Elements in Mongolian Medicine Bateri by ICP-AES[J].Chinese Journal of Inorganic Analytical Chemistry,2016,6(4):1-3. |
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| Authors: | BAO Lidao WU Lanqiqige and ZHAO Yuying |
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| Institution: | School of Stomatology of Chifeng University, Chifeng, Inner Mongolia 024000, China,School of Stomatology of Chifeng University, Chifeng, Inner Mongolia 024000, China and College of Chemistry and Chemical Engineering, Inner Mongolia University for the Nationalities Natural Product Development and Waste Utilization, Tongliao, Inner Mongolia 028043,China |
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| Abstract: | A rapid and accurate method for the determination of multiple elements in Mongolian Medicine Bateri was developed. The contents of 17 kinds of major and minor elements and heavy metal elements were simultaneously measured by ICP-AES, and the recovery experiments were also carried out. The results indicated that Ca, P and K had high concentrations, the nutrient elements such as Fe and Mg were rich in Mongolian Medicine Bateri, and the contents of every heavy metal element, such as Pb and Cd were lower than those obtained in national standards of Bateri. The average recovery rate of each element was 95.8%-103.1% with the relative standard deviation (RSD) of 1.7%-3.3%. The method is accurate and reliable, and is suitable for simultaneous determination of multiple elements in Mongolian Medicine Bateri. |
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