Synthesis and structure of bis(monohaloacetates) of tris(5-bromo-2-methoxyphenyl)antimony |
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| Authors: | V V Sharutin O K Sharutina D S Tolstoguzov |
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| Institution: | 1. National Southern Ural Research State University, pr. Lenina 76, Chelyabinsk, 454080, Russia
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| Abstract: | Tris(5-bromo-2-methoxyphenyl)antimony bis(monohaloacetates) (5-Br)(2-MeO)C6H3]3SbOC(O)CH2X]2, X = Cl (I), Br (II), I (III) have been synthesized by the reaction of tris(5-bromo-2-methoxyphenyl)antimony with chloro-, bromo-, and iodoacetic acids in the presence of hydrogen peroxide. According to X-ray analysis the antimony atom in I–III has a distorted trigonal-bipyramidal coordination. |
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