| 二苄基锡双(四氢吡咯荒酸酯)的合成、表征和晶体结构 |
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| 引用本文： | 尹汉东,王传华,马春林,朱德忠.二苄基锡双(四氢吡咯荒酸酯)的合成、表征和晶体结构[J].无机化学学报,2002,18(8):819-822. |
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| 作者姓名： | 尹汉东 王传华 马春林 朱德忠 |
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| 作者单位： | 聊城师范学院化学系,聊城,252059 |
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| 基金项目： | 教育部骨干教师基金，山东省自然科学基金资助项目(No.Y2000B08) |
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| 摘 要： | Dibenzyltin bis(dithiotetrahydropyrrolocarbamate) was synthesized by the reaction of dibenzyltin dichloride with dithiotetrahydropyrrolocarbamate. The compound was characterized by elemental analysis, IR, 1H NMR and MS. and the crystal structure was determined by X-ray single crystal diffraction. The crystal belongs to or-thorhombic with space group Pccn, a=2.1665(6)nm, b=0.9932(3)nm, c=1.1979(3)nm,α=90°,β=90°,γ=90°,Z=2,V=2.5777(12)nm3,Dc=1.529g·cm-3,μ(MoKα)=1.330mm-1,F(000)=1208,R1=0.0341, wR2=0.0627. In the crystals, the structures consist of discrete molecules in which the tin atom is six-coordinate in a distorted octahedron configuration. CCDC: 179919.
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| 关 键 词： | 二苄基锡双(四氢吡咯荒酸酯) 合成 晶体结构 |
| 修稿时间： | 2002年3月2日 |
Synthesis, Characterization and Crystal Structure of Dibenzyltin Bis(dithiotetrahydropyrrolocarbamate) |
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| YIN Han-Dong,WANG Chuan-Hu,MA Chun-Lin and ZHU De-Zhong.Synthesis, Characterization and Crystal Structure of Dibenzyltin Bis(dithiotetrahydropyrrolocarbamate)[J].Chinese Journal of Inorganic Chemistry,2002,18(8):819-822. |
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| Authors: | YIN Han-Dong WANG Chuan-Hu MA Chun-Lin and ZHU De-Zhong |
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| Institution: | Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059,Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059,Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059 and Department of Chemistry, Liaocheng Teachers University, Liaocheng 252059 |
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| Abstract: | |
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| Keywords: | dibenzyltin dithiotetrahydropyrrolocarbamate synthesis crystal structure |
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