Dimerization of acetylacetone upon the action of 3,6-di-tert-butyl-ortho-benzoqutnone and tetrafluorosilane |
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| Authors: | A. K. Chekalov D. S. Yufit A. I. Prokofev V. B. Vol'eva Yu. T. Struchkov M. I. Kabachnik |
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| Affiliation: | (1) A. N. Nesmeyanov Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, USSR |
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| Abstract: | ![]()
1,3,5,7-Tetramethyl- 2,4,6,8-tetraoxaadamantane was obtained by the dimerization of acetylacetone in the presence of 3,6-di-tert-butyl-orthobenzoquinone and tetrafluorosilane. An x-ray diffraction structural analysis was carried out for the tetraoxaadamantane obtained.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 10, pp. 2375–2377, October, 1989. |
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