Synthesis and X-ray analysis of 1-((1S)-phenylethyl)-azetidine-(2R)-piperidinamide |
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| Authors: | R. de Gelder J. M. M. Smits W. A. J. Starmans L. Thijs B. Zwanenburg |
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| Affiliation: | (1) Department of Inorganic Chemistry, Nijmegen SON Research Center, University of Nijmegen, Toernooiveld, 6525 ED Nijmegen, The Netherlands;(2) Department of Organic Chemistry, Nijmegen SON Research Center, University of Nijmegen, Toernooiveld, 6525 ED Nijmegen, The Netherlands |
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| Abstract: | The crystal and molecular structure of a new azetidine-2-carboxylic amide derivative is described. The structure was solved by direct methods and refined by least squares methods toR1=0.0393 for 4264 reflections (withI>2 (I)) The structure consists of two independent molecules which are chemically the same with slight differences in geometry. Crystal data: C17H24N2O, monoclinic, space groupP21,a=8.3782(4),b=20.0342(13),c=9.7769(8) Å,  =109.687(6)°,V=1545.1(2)Å3,Z=4. |
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| Keywords: | Crystal structure chiral auxiliaries |
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