CRYSTAL AND MOLECULAR STRUCTURE OF cis-ISOMER OF 1-N-PROPYL-3-iso-PHOPYL-2-PHENYL-4-ETHOXY-4,5-DIOXO-2-THIO-1,3,2,4-DIAZADIPHOSPHOLANE |
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摘 要: | <正> PhP(S)N(C3H5-i)-PO(OEt)CON(C3H5) Mr=358.34, monoclinic, space group P21/c, a=8.654(3), b=15.390(2), c=15.235(3)A,β=101.48(2)°;Z=4, Dx=1.20g/cm3, λ(No Kα)=0.71069A,μ=3.24cm-1. The final refinement converged with R=0.047 and Rw=0.051 for 1326 observed independent reflections.
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CRYSTAL AND MOLECULAR STRUCTURE OF cis-ISOMER OF 1-N-PROPYL-3-iso-PHOPYL-2-PHENYL-4-ETHOXY-4,5-DIOXO-2-THIO-1,3,2,4-DIAZADIPHOSPHOLANE |
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Abstract: | PhP(S)N(C_3H_5-i)-PO(OEt)CON(C_3H_5) Mr=358.34, monoclinic, space group P21/c, a=8.654(3), b=15.390(2), c=15.235(3)A,β=101.48(2)°;Z=4, Dx=1.20g/cm3, λ(No Kα)=0.71069A,μ=3.24cm-1. The final refinement converged with R=0.047 and Rw=0.051 for 1326 observed independent reflections. |
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