Analysis of siloxane pyrolysis products by cryo-GC/FT-IR and GC/MS |
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Authors: | S Wachholz U Just F Keidel H Gei?ler and K K?ppler |
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Institution: | (1) Federal Institute of Materials Research and Testing, Unter den Eichen 87, D-12205 Berlin, Germany;(2) Technical University Dresden, Mommsenstrasse 13, D-01069 Dresden, Germany |
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Abstract: | On line measurements of infrared and mass spectra of siloxane pyrolysis products separated by gas chromatography are described. The FT-IR absorbance spectra have been recorded from the eluates trapped as small spots on a moving window held at 77 K. Three of the main compounds separated were selected for FT-IR identification performed by comparing the spectra with GC/MS data and by spectral searching using a library of compounds measured under the same conditions.Dedicated to our most honourable teacher Professor Dr. H. Kriegsmann on the occasion of his 70th birthday |
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