Synthesis of a dicyclobutylideneethane derivative via sequential palladium-catalyzed Miyaura borylation and Suzuki coupling |
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| Authors: | George W. KabalkaMin-Liang Yao |
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| Affiliation: | Departments of Chemistry and Radiology, The University of Tennessee, Knoxville, TN 37996-1600, USA |
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| Abstract: | An efficient synthesis of a dicyclobutylideneethane derivative was achieved using a palladium-catalyzed reaction of a substituted (bromomethylene)cyclobutane with bis(pinacolato)diboron. The reaction mechanism was investigated in detail. The Suzuki cross-coupling reaction of a (bromomethylene)cyclobutane with arylboronic acid was also achieved. |
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| Keywords: | Suzuki coupling borylation synthesis dicyclobutyldieneethane |
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