One-pot assembly of tricyclo[6.2.1.0(1,6)]undecan-4-one and related polycyclic compounds by tandem electroreductive cyclization |
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| Authors: | Toyota Masahiro Ilangovan Andivelu Kashiwagi Yoshitomo Ihara Masataka |
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| Affiliation: | Department of Organic Chemistry, Graduate School of Pharmaceutical Sciences, Tohoku University, Aobayama, Sendai 980-8578, Japan. |
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| Abstract: | [reaction: see text] Electroreductive tandem cyclization of 4-allyl-4-(2-bromoprop-2-en-1-yl)cyclohex-2-en-1-one to tricyclo[6.2.1.0(1,6)]undecan-4-one has been demonstrated. This protocol represents an attractive alternative to conventional tandem radical cyclization. |
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