Determination of uranium by XRF analysis following its preconcentration with some organic precipitants |
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Authors: | V Spěvá?ková J Jhn M Pra?ská |
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Institution: | 1. Department of Nuclear Chemistry, Technical University of Prague, B?ehová 7, 115 19, Prague 1, (Czechoslovakia)
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Abstract: | The determination of uranium in natural waters by XRF analysis after its preconcentration with some organic precipitants is described.109Cd source is used for the excitation of L-series X-rays of uranium. Separation yield, kinetics of coprecipitation and the possibility of preparing thin-layer samples for XRF analysis were studied in detail for uranium concentration with α-nitroso-β-naphtol, methylene blue with ammonium thiocyanate, tannin with urotropine and other precipitants. A procedure using coprecipitation of uranium with α-nitroso-β-naphtol from 500 ml samples of surface or waste, waters is proposed. |
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