Structural study of highly porous nanocomposite aerogels |
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Institution: | Dipartimento di Scienze Chimiche and INSTM, Università di Cagliari, S.S. 554 bivio per Sestu, Monserrato, CA, Italy;Institute of Physics, Academy of Sciences of the Czech Republic, Prague, Czech Republic |
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Abstract: | The structural properties of CoFe2O4–SiO2 highly porous nanocomposite aerogels have been investigated by X-ray Absorption Spectroscopy and Transmission Electron Microscopy techniques. The aerogels are obtained by supercritical drying of composite gels obtained using a two step procedure where fast gelation is achieved using urea in the second step. The formation of CoFe2O4 nanocrystals in the silica matrix begins after calcination at 750 °C of the parent aerogel and is complete after calcination at 900 °C, while the high porosity of the sample is mostly retained. |
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