| 相转移催化法合成1-O-(2',4'-二硝基苯)-2-乙酰氨基-β-D-葡萄糖苷 |
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| 引用本文： | 熊兴泉,郭振楚,欧阳文竹.相转移催化法合成1-O-(2'',4''-二硝基苯)-2-乙酰氨基-β-D-葡萄糖苷[J].化学研究与应用,2003,15(6):817-818. |
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| 作者姓名： | 熊兴泉 郭振楚 欧阳文竹 |
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| 作者单位： | 湖南科技大学化学化工系,湖南,湘潭,411201 |
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| 基金项目： | 湖南省重点学科资助项目(湘财政[2002]8号) |
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| 摘 要： | This paper reports that in the presence of cetyhrimethyl ammonium bromide as phase transfer catalyst, D-glucosamine hydrochloride reacts with 2,4-dinitrophenol to synthesize 1-O-(2' ,4'-dinitrophenyl)-2-acetamido-β-D-glucoside. Chemical structure of the new compound was confirmed by elemental analysis, IR and UV.
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| 关 键 词： | 相转移催化法 合成 1-O-（2’，4’-二硝基苯）-2-乙酰氨基-β-D-葡萄糖苷 糖甘化 |
| 文章编号： | 1004-1656(2003)06-0817-02 |
| 修稿时间： | 2003年3月24日 |
Synthesis of 1-O-(2',4'-dinitrophenyl)-2-acetamido-β-D-glucoside by phase-transter catalysis method |
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| XIONG Xing-quan,GUO Zhen-chu,OUYANG Wen-zhu.Synthesis of 1-O-(2'',4''-dinitrophenyl)-2-acetamido-β-D-glucoside by phase-transter catalysis method[J].Chemical Research and Application,2003,15(6):817-818. |
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| Authors: | XIONG Xing-quan GUO Zhen-chu OUYANG Wen-zhu |
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| Abstract: | |
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| Keywords: | D-glucosamine hydrochloride 2 4-dinitrophenol phase transfer catalysis glucosidation synthesis |
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