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Temperature program optimization by computer simulation for the capillary GC analysis of fatty acid methyl esters on biscyanopropyl siloxane phases |
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| Authors: | Erkki Sippola Frank David Pat Sandra |
| Abstract: | The selectivity of capillary columns coated with biscyanopropyl siloxane stationary phases for the separation of fatty acid methyl esters has been optimized by means of computer-assisted column temperature optimization software. Temperature programming rates yielding the highest resolution in the shortest analysis time were selected for split, splitless, and on-column injection operated in the constant pressure and pressure programmed modes. |
| Keywords: | Capillary GC Biscyanopropyl siloxane phases Temperature program optimization Computer simulation (Drylab GC) Fatty acid methyl esters Electronic pressure control |