| Co(II)(C7H7O2N)2(C12H12N2)2微晶粉体的水热合成及表征 |
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| 引用本文： | 姜敏.Co(II)(C7H7O2N)2(C12H12N2)2微晶粉体的水热合成及表征[J].人工晶体学报,2006,35(2):319-321. |
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| 作者姓名： | 姜敏 |
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| 作者单位： | 陕西理工学院化学系,汉中,723001 |
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| 基金项目： | 陕西理工学院科研专项基金资助项目(SLG0429) |
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| 摘 要： | 本文以对氨基苯甲酸和联苯胺为配体,通过水热合成制备Co(II)的配合物,得到Co(II)(C7H7O2N)2(C12H12N2)2(C7H7O2N= p-aminobenzoic acid, p-abza, C12H12N2= Benzidine)深蓝色微晶颗粒.通过元素分析、IR等方法对配合物进行了表征,并通过TG分析对该配合物的热稳定性及热分解机理做了初步探讨.
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| 关 键 词： | 对-氨基苯甲酸 联苯胺 水热合成 晶体 |
| 文章编号： | 1000-985X(2006)02-0319-03 |
| 修稿时间： | 2005年9月5日 |
Co(II)(C7H7O2N)2(C12H12N2)2 Powder Crystal by Hydrothermal Method and Characteration |
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| JIANG Min.Co(II)(C7H7O2N)2(C12H12N2)2 Powder Crystal by Hydrothermal Method and Characteration[J].Journal of Synthetic Crystals,2006,35(2):319-321. |
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| Authors: | JIANG Min |
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| Abstract: | A deep-blue crystal Co(II)(C_7H_7O_2N)_2(C_(12)H_(12)N_2)_2 was synthesized by the hydrothermal method,and characterized by elemental and IR analyses.The thermal decomposition mechanism of the compound was also discussed based on the TG curves.Its structure is unknown yet at present because of the too tiny shape of the title complex. |
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| Keywords: | p-aminobenzoic acid benzidine hydrothermal synthesis crystal |
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