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排序方式: 共有915条查询结果,搜索用时 15 毫秒
1.
AbstractHerein the bioaccessibility of Mn, Cu, Zn, Cd, and Pb, selected from essential and toxic elements, was determined in commercially sold vegetable purees intended for infant and toddler consumption. Chemical fractionation studies using water, acetone, diethyl ether, chloroform:methanol, and n-hexane were employed to predict the importance of the protein and lipid parts of a matrix to assess the bioaccessibility data. In addition, in-vitro gastrointestinal digestion was performed to determine the bioaccessibility of the elements using a five level, three factor central composite design (CCD) to maximize the elemental solubility. The total elemental concentrations in all of the fractions were determined by inductively coupled plasma – mass spectrometry (ICP-MS). Based on the consumption of one jar of vegetable/rice-based baby food, Zn was 1.3% of the recommended dietary allowance and Mn was 4.2% of the adequate intake level, while Cu was almost 100% of the adequate intake level. Additionally, Pb was always below the detection limit and Cd was sometimes under the detection limit for the percent bioaccessibility. However, in some samples, Cd was as high as 80% of the tolerable weekly intake level depending on the body weight. 相似文献
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The aim of this study was ultrasound assisted removal of Ceftriaxone sodium (CS) based on CCD model. Using sonochemical synthesized Bi2WO6 implanted on graphitic carbon nitride/Multiwall carbon nanotube (g-C3N4/MWCNT/Bi2WO6). For this purpose g-C3N4/MWCNT/Bi2WO6 was synthesized and characterized using diverse approaches including XRD, FE-SEM, XPS, EDS, HRTEM, FT-IR. Then, the contribution of conventional variables including pH, CS concentration, adsorbent dosage and ultrasound contact time were studied by central composite design (CCD) under response surface methodology (RSM). ANOVA was employed to the variable factors, and the most desirable operational conditions mass provided. Drug adsorption yield of 98.85% obtained under these defined conditions. Through conducting five experiments, the proper prediction of the optimum point were examined. The respective results showed that RSD% was lower than 5% while the t-test confirmed the high quality of fitting. Langmuir isotherm equation fits the experimental data best and the removal followed pseudo-second order kinetics. The estimation of the experimentally obtained maximum adsorption capacities was 19.57 mg.g− of g-C3N4/MWCNT/Bi2WO6 for CS. Boundary layer diffusion explained the mechanism of removal via intraparticle diffusion. 相似文献
4.
介绍了一个本科生的仪器分析实验——光纤光谱仪的多样化组装及应用。利用光源、光纤和电荷耦合器件检测器等部件,组装出紫外-可见光谱仪、分子荧光光谱仪、近红外光谱仪、拉曼光谱仪和激光诱导荧光光谱仪。通过本实验,不仅能够拓展传统光学实验的内容,而且可以通过自己动手组装仪器,培养学生的专业实践能力和知识应用能力。 相似文献
5.
Effect of the nonlinearity of the CCD in Fourier transform profilometry on spectrum overlapping and measurement accuracy 下载免费PDF全文
In Fourier transform profilometry (FTP), we must restrain spectrum overlapping caused by the nonlinearity of the charge coupled device (CCD) and increase the measurement accuracy of the object shape. Firstly, the causes of producing higher-order spectrum components and inducing spectrum overlapping are analysed theoretically, and a simple physical explanation and analytical deduction are given. Secondly, aiming to suppress spectrum overlapping and improve measurement accuracy, the influence of spatial carrier frequency of projection grating on them is analysed. A method of increasing the spatial carrier frequency of projection grating to restrain or reduce the spectrum overlapping significantly is proposed. We then analyze the mechanism of how the spectrum overlapping is reduced. Finally, the simulation results and experimental measurements verify the correction of the proposed theory and method. 相似文献
6.
TDICCD拼接相机的像元响应非均匀性校正方法 总被引:1,自引:0,他引:1
为了解决光学TDICCD成像系统在拼接模式下的像元响应非均匀性问题,研究了TDICCD像元校正的原理和实现方法。提出了视频处理器在不同增益、不同偏置和TDICCD在不同积分时间下进行像元校正的方法,设计了在现场可编程门阵列(FPGA)平台下进行了程序实现和验证的方法。实验数据分析表明:成像系统单片TDICCD的非均匀性由4.72%降低到0.27%,恶劣环境下TDICCD成像系统的图像非均匀性可以降低2.55%。该像元级校正算法简单,可靠性高,能够满足星上成像的要求;在不同的增益、偏置和积分时间下能够很好地解决TDICCD成像系统的像元响应非均匀性问题。 相似文献
7.
为了提高像移测量精度,针对机载航空摆扫相机提出一种坐标变换法和图像相关法相结合的像移测量方法。利用坐标变换法得到初始像移速度,利用图像联合变换相关法对像移速度残差进行补偿。联合图像通过一个面阵CCD获得,该面阵CCD放置在相机焦平面上并与成像线阵TDI CCD平行,其输出的当前图像与参考图像合并构成联合图像进行二维空间联合变换相关运算,得到像移修正矢量。对该矢量分别在相机摆扫方向和载机飞行方向进行分解,从而得到摆扫像移和前向像移的修正量。仿真实验结果表明,在输入图像信噪比为4 dB时,像移测量误差在0.1 pixel以内。 相似文献
8.
根据激光线阵CCD检测技术原理,提出一种快速、高准确度的轧辊辊型检测方法,阐述了系统组成与检测过程.针对辊型检测过程中易出现的轴线偏移现象,从垂直检测平面和平行检测平面两个方向采取补偿措施,有效地提高了系统检测准确度.同时检测系统对CCD信号进行处理时,采用浮动阈值法,有效降低噪音对CCD成像质量的影响,保证了系统的分辨率与检测准确度.实验证明,系统的检测准确度可达到实际生产过程中辊型检测的要求,为实现辊型在线检测的高速、高准确度、高自动化提供了一种新的研究方法. 相似文献
9.
线阵CCD已广泛应用于在线检测、图像识别等系统,目前高帧率采集系统多在200~500Hz之间。高速线阵CCD采集系统,如1K甚至10KHz以上的采集要求,设计难度大,电路实现复杂,需要专用处理器,产品成本高,提出了一种采用并行高速FPGA驱动线阵CCD,通过常规分立元件完成模拟信号处理,实现数字信号实时传输的方案。该方案不仅简化了硬件设计上的难度,在同等性能情况下,可实现每秒万帧的高速采样,大幅度降低了成本。方案选用Altera FPGA作为控制核心,实现高速信号采集的同时,在片上实现一定的图像算法,不仅加速了图像处理速度,同时降低了计算机的处理压力。最后,本电路通过USB2.0接口,完成数据的实时传输。设计具有高帧率、高灵敏度、性能稳定,便携使用等特点,同时还有一定的通用性,已应用于一些光学系统中。 相似文献
10.
《Optik》2014,125(24):7136-7139
The idea of using spatial filtering method to measure velocity of vehicles for an inertial navigation system is put forward. Corresponding optical system, including a 532 nm solid-state laser as active illumination, is established. A 17.92 mm × 14.34 mm area charge coupled device (CCD) is employed both as detector and as spatial filter. The spatial filtering characteristics are theoretically analyzed using a power spectral density function. The spatial filtering operation of CCD is performed fully by software. Therefore, the parameters of the spatial filter, such as the size and the number of spatial period, are changeable. In addition, the CCD is arranged as two differential spatial filters without any other additional elements. Experiments are carried out to examine the feasibility of CCD as two differential spatial filters and the influence of the number of spatial period on the signal frequency. The results indicate that the more number of spatial period the more accurate measurements can be obtained, and show that the relation between signal frequency and velocity has good linearity. So this velocimeter is suitable to provide velocity information for a vehicle self-contained inertial navigation system. 相似文献