共沉淀法制备Y_2O_2S∶Eu~(3+),Mg~(2+),Ti~(4+)红色长余辉材料

用共沉淀法制备了Y2O2S∶Eu3 ,Mg2 ,Ti4 红色长余辉材料。测量了材料的电子显微形貌、晶体结构和发射光谱。通过与固相法制备的Y2O2S∶Eu3 ,Mg2 ,Ti4 长余辉材料比较,发现两种方法都可以制备粒度基本相同的纯相Y2O2S基质晶体,但共沉淀法样品的颗粒结构更松散。研究了Eu3 浓度对两种方法制备样品的谱线发射强度的影响,通过比较共沉淀法和高温固相法制备的样品中Eu3 的5D1→7F3较高能级跃迁的587.6 nm谱线强度随Eu3 浓度的变化,发现共沉淀法更有利于Eu3 均匀进入Y2O2S基质晶格而形成有效的发光中心。     

The Design of a 25-Barrel Pellet Injector with Cycle Refrigerator for the HL-2A Device

In the study of nuclear fusion, the conventional fuelling of plasma is edge gas puffing, however many experiments indicated that the fuelling efficiency of gas puffing usually degraded with increase of heat power leading the density profile of plasma control     

Dependence of Isospin Fractionation on Beam Energy in Heavy Ion Collisions at Intermediate Energies

We investigated the dependence of isospin fractionation degree (N/Z)n/ (N/Z)Nfrag on the beam energy by using the isospin dependent quantum molecular dynamics model (IQMD). The (N/Z)n and (N/Z)Nfrag are the neutron proton ratio of nucleon emission (gas phase) and that of fragment emission (liquid phase) respectively. The calculated results show that (N/Z)n / (N/Z)Nfrag enhances with increasing the beam energy due to the increase of excitation energy of colliding system. But above properties is only occurred in the definiteenergy region.     

电场喷射活细胞

一般人使用喷墨打印机来打印文件和图片＋这种技术将细小的彩色墨滴从喷嘴中挤压出来．然而，在电子学和医学中正越来越多地用这种技术产生小体积的液滴．例如，使用压电晶体从一根针头中挤压出含有细胞的溶液，产生活细胞的二维和三维图像．但是细胞液滴的大小受到针头直径大小的限制＋因而这种方法不能产生小于100μm同左右的液滴．这意味着很难制成带有细微特征的小的生物组织．     

Characteristics of Nd：GdVO4 Laser with Different Nd-Doping Concentrations

We report the properties of a compact diode-pumped continuous-wave Nd：GdV04 laser with a linear cavity and different Nd-doped laser crystals. In a 0.2at.% Nd-doped Nd：GdVO4 laser, 1.54 W output laser power is achieved at 912nm wavelength with a slope efficiency of 24.8% at an absorbed pump power of 9.4W. With 0.3at.% Nd-doping concentration, we can obtain the either single-wavelength emission at 1064nm or 912nm or the dual-wavelength emission at 1064nm and 912nm by controlling the incident pump power. From an incident pump power of 11.6 W, the 1064nm emission between ^4Fa/2 and ^4I11/2 is suppressed completely by the 912nm emission between ^4Fa/2 and ^4I9/2. We obtain 670 mW output of the 912nm single-wavelength laser emission with a slope efficiency of 5.5% by taking an incident pump power of 18.4 W. Using a Nd：GdV04 laser with 0.4at.% Nd-doping concentration, we obtain either the single-wavelength emission at 1064nm or the dual-wavelength emission at both 1064nm and 912nm by increasing the incident pump power. We observe a strong competition process in the dualavelength laser.     

低进汽压力下超音速两相流升压特性实验研究

本文采用实验方法研究了进汽压力为0.2 MPa以下时,由蒸汽喷嘴、混合腔及相应的阀门和管道组成超音速汽液两相流升压加热装置的运行特性。实验表明在进汽压力为0.1 MPa-0.2 MPa时,超音速汽液两相流升压加热装置都可稳定可靠地运行,且升压效果明显,可满足电力、供暖、轻工等许多行业蒸汽加热的要求。     

铈锆复合氧化物氧非化学计量值的测定

1引言采用氨水共沉淀法制备出CexZr1-xO2-δ复合氧化物。用氧化还原返滴定法测定样品氧非化学计量值,并采用热重法进行方法比对实验以考察方法的可行性。结果表明,本方法可得到准确CexZr1-xO2-δ的氧非化学计量值δ的测定值,并分别对不同原子比的CexZr1-xO2-δ复合氧化物样品的     

氯离子柱撑水滑石共沉淀法合成反应动力学

根据氯离子型层状复合氢氧化物(LDH-Cl)制备过程中溶液浓度变化的监测结果和不同反应进程时产物的EDS、IR、XRD、TEM、TG-DTA表征结果,研究了合成LDH-Cl的共沉淀反应动力学特征及机理.实验结果表明, LDH-Cl的生成符合多核层表面反应动力学模型;反应过程中LDH的晶胞参数c从2.421 nm变为2.399 nm,通道高度h由0.3321 nm减小为0.3228 nm,粒子直径Da由6.40 nm增大为15.16 nm, Dc由7.43 nm增大到10.93 nm,纵横比由0.86增大为1.39; IR和TG-DTA特征变化表明了层板对阴离子作用的强度和层板的结构稳定性随反应进程而提高.     

纳米PbSnO3的制备及其燃烧催化性能的研究

Nanocomposite PbSnO₃was synthesized by coprecipitation method , and its phase evolution process was investigated. The particle size, crystal form, and phase of samples were determined with XRD, TEM and EDS. The catalytic actiyity of sample on the thermal decomposition of RDX was investigated by DSC. The results show that nanocomposite PbSnO₃with the diameter of 9 nm can be obtained by calcining at 600 ℃ for 2 h, which crystal is cubic (pyrochlore type). The catalytic actiyity of nanocomposite PbSnO₃on the thermal decomposition of RDX is much higher than that of normal PbSnO₃. The nanocomposite PbSnO₃can decrease the peak temperature of thermal decomposition of RDX from 240.1 ℃ to 236.5 ℃, and the decomposition enthalpy ΔH of RDX increases 722 J·g^-1 （about 70%）.     

LaNi4Fe催化合成氨反应性能的研究

用冶金法、还原扩散法、共沉淀法制得了LaNiFe,并对其催化合成氨反应性能进行了研究。实验结果表明:还原扩散法,共沉淀法制得的LaNi_4Fe催化活性均比冶金法好。X—射线分析指出LaNi_4Fe在合成氨反应过程中变为Ni_4Fe和LaN。