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The protected ceramide: N‐((2S,3S,4R)‐3,4‐bis(benzyloxy)‐1‐hydroxyoctadecan‐2‐yl)tetracosanamide, was attempted to introduce a triflate as a leaving group followed by a nucleophilic substitution with azido group in one‐pot manner. Unexpectedly, the oxazole ring formed via a thermodynamically favored intramolecular cyclization was opened to generate the original ceramide by triflic acid. In addition, the residual acid promoted a formylation of the primary hydroxy group in DMF. 相似文献
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无损残余应力测量及其新技术 总被引:1,自引:0,他引:1
简述及比较了主要的残余应力无损测量技术,重点为磁力法,并介绍一台新的磁力仪MAPS,且对MAPS及传统磁力仪作了比较,同时以X射线及中子衍射得到的结果验证了MAPS的可靠性,也介绍了文献上较少见的火车钢轨残余应力分布图。 相似文献
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本文提出了反常作用的μ荷观点,μ荷不仅是一种反映μ-e禁戒性的量子数,而且是反常作用的承担者。在此观点下,讨论了轻子结构和μ-e质量差,得到了关于轻子结构的一些普遍定理。例如,证明了电子的反常作用和电磁作用形状因子相同等。在讨论轻子结构的基础上,得到了将μ-e质量差和轻子的电磁结构相联系的公式,证明了主要由于电磁作用干涉产生的μ荷-μ矩作用是反常作用自能的主要部分,它是负值,故是电子参与反常作用。利用电子的电磁结构数据能合理地解释μ-e质量差,而后者也提供了有关电子电磁结构的进一步知识。 相似文献
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Based on the microscopic two velocity difference model, a macroscopic model called speed viscous continuum model is developed to describe traffic flow. The relative velocities are added to the motion equation, which leads to viscous effects in continuum model. The viscous continuum model overcomes the backward travel problem, which exists in many higher-order continuum models. Nonlinear analysis shows that the density fluctuation in traffic flow leads to density waves. Near the onset of instability, a small disturbance could lead to solitons described by the Korteweg-de Vries-Burgers (KdV-Burgers) equation, which is seldom found in other traffic flow models, and the soliton solution is derived. 相似文献