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1.
A temperature control unit was implemented to vary the temperature of samples studied on a commercial Mobile Universal Surface Explorer nuclear magnetic resonance (MOUSE-NMR) apparatus. The device was miniaturized to fit the maximum MOUSE sampling depth (25 mm). It was constituted by a sample holder sandwiched between two heat exchangers placed below and above the sample. Air was chosen as the fluid to control the temperature at the bottom of the sample, at the interface between the NMR probe and the sample holder, in order to gain space. The upper surface of the sample was regulated by the circulation of water inside a second heat exchanger placed above the sample holder. The feasibility of using such a device was demonstrated first on pure water and then on several samples of bread dough with different water contents. For this, T1 relaxation times were measured at various temperatures and depths and were then compared with those acquired with a conventional compact closed-magnet spectrometer. Discussion of results was based on biochemical transformations in bread dough (starch gelatinization and gluten heat denaturation). It was demonstrated that, within a certain water level range, and because of the low magnetic field strength of the MOUSE, a linear relationship could be established between T1 relaxation times and the local temperature in the dough sample.  相似文献   
2.
Abdi  Ahmad  Cornuéjols  Gérard  Huynh  Tony  Lee  Dabeen 《Mathematical Programming》2022,192(1-2):29-50
Mathematical Programming - A clutter is k-wise intersecting if every k members have a common element, yet no element belongs to all members. We conjecture that, for some integer $$k\ge 4$$ , every...  相似文献   
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1,8-Napthalimides (NIs) have been widely used as fluorescent molecules in biological, chemical, and medical fields because NIs shows high stability and various fluorescence properties under different conditions. However, NIs typically display a fluorescence emission wavelength in the range of 350 – 550 nm which can be notably interfered with by autofluorescence in living cells, significantly limiting their bio-applications. Moreover, low solubility in aqueous media is another major limitation for NIs. In this project, four derivatives of NIs (1–4) have been synthesized via an aromatic nucleophilic substitution reaction and their photophysical properties have been investigated in various media (water, MeOH, MeCN, DMSO, EtOAc, and THF). All of these derivatives (1–4) show a long emission wavelength around 600 nm and high solubility in polar solvents. Particularly molecules (14) show the longest emission (624–629 nm) in water and the fluorescence intensity is not significantly varied in the range of pH 4–11. These unique features, long emission wavelength, high solubility, and high stability in difference pH media, will allow these derivative (14) to be used as excellent labeling reagents in the biological system.

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4.
Ghavanloo  Esmaeal  Fazelzadeh  S. Ahmad 《Meccanica》2021,56(7):1819-1829

In this paper, an analytical matrix method is presented to drive closed-form characteristic equations for natural frequencies of finite monoatomic and diatomic metamaterials with various boundary conditions. Here, we extend the matrix method introduced by Louck for monoatomic lattice chains. The proposed method is used to calculate the vibration frequencies of the monoatomic metamaterials with fixed–fixed, fixed-free and free-free boundary conditions. In addition, the natural frequencies of fixed–fixed diatomic metamaterials are calculated. The existence of band gaps in the frequencies of the metamaterials is numerically shown.

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5.
Mu  Xiaojie  Jiang  Daqing  Hayat  Tasawar  Alsaedi  Ahmed  Ahmad  Bashir 《Nonlinear dynamics》2021,103(2):2081-2096
Nonlinear Dynamics - The mathematical model with time delay is often more practical because it is subject to current and past state. What remains unclear are the details, such as how time delay and...  相似文献   
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Acta Mathematica Sinica, English Series - For a finite group G, the power graph $$\cal{P}(G)$$ is a simple connected graph whose vertex set is the set of elements of G and two distinct vertices x...  相似文献   
8.

This article studies buoyancy-driven natural convection of a nanofluid affected by a magnetic field within a square enclosure with an individual conductive pin fin. The effects of electromagnetic forces, thermal conductivity, and inclination angle of pin fin were investigated using non-dimensional parameters. An extensive sensitivity analysis was conducted seeking an optimal heat transfer setting. The novelty of this work lies in including different contributing factors in heat transfer analysis, rigorous analysis of design parameters, and comprehensive mathematical analysis of solution domain for optimization. Results showed that magnetic strength diminished the heat transfer efficacy, while higher relative thermal conductivity of pin fin improved it. Based on the problem settings, we also obtained the relative conductivity value in which the heat transfer is optimal. Higher sensitivity of heat transfer was, though, noticed for both magnetic strength and fin thermal conductivity in comparison to fin inclination angle. Further studies, specifically with realistic geometrical configurations and heat transfer settings, are urged to translate current findings to industrial applications.

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