排序方式: 共有56条查询结果,搜索用时 125 毫秒
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以双三氟甲烷磺酰亚胺离子([NTf2]-)为阴离子,合成阳离子烷基取代不同(C1、C2和C4)的硅烷基咪唑离子液体,以其为固定相制备气相色谱填充柱。 硅烷基咪唑离子液体为强极性固定相;阳离子结构影响固定相的热稳定性、极性和分离性能。 在这些离子液体固定相中,1-丁基-3-[(3-三甲氧基硅基)-丙基]咪唑双三氟甲烷磺酰亚胺([PBIM]NTf2)对Grob试剂分离性能较好。 利用溶剂化作用参数模型,评价[PBIM]NTf2固定相特性,研究固定相-组分分子之间相互作用机制;同时考察[PBIM]NTf2色谱柱对不同类型化合物的分离性能。 结果表明,[PBIM]NTf2固定相主要作用力是氢键碱性和偶极作用,对烷烃、醇、酯和胺等不同类型的样品组分表现出良好的分离能力。 相似文献
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Multi-wavelength seed laser can mitigate stimulated Brillouin scattering (SBS) and improve the output power of the narrow-linewidth fiber amplifier. In this present study~ coherent combining of two fiber amplifiers seeded by a multi-wavelength laser is proposed and demonstrated using stochastic parallel gradient descent (SPGD) algorithm. The long-exposure visibility of the far field interference pattern is increased from 0.15 to 0.97 when the system evolves from open-loop to closed-loop. The feasibility of coherent combining of fiber amplitlers seeded by multi-wavelength seed laser is validated. 相似文献
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We demonstrate the coherent beam combination of eight Watt-level polarization-maintained fiber amplifiers. The phase control signal of each amplifier is generated by running a stochastic parallel gradient descent algorithm on a digital signal processor (DSP). The experimental result shows that the whole system in close-loop performs well for long-time observation. Energy encircled in the target pinhole is 6.68 times more than that in open-loop. The combination efficiency is as high as 84.5%. 相似文献
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由于受到受激布里渊散射(SBS)等非线性效应的限制,单频激光放大器的功率在百瓦量级,以非单频激光多波长激光作为种子源能够有效地抑制SBS并提高放大器功率.与单频激光相干合成相比,非单频率、多波长激光的相干合成有望将输出激光功率成量级地提高.基于随机并行梯度下降(stochastic parallel gradient descent,SPGD)算法,实现了四波长激光的相干合成.在系统闭环时,四路多波长激光合成后的主瓣能量能够提高3倍,达到理想值的75%.验证了多波长、非单频激光相干合成的可行性,为高功率相干合成的发展提供了新的途径. 相似文献
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Beam quality and power scalability analyses for various multicore fiber lasers (MFL) are presented. In-phase complex amplitude and corresponding far-field intensity distribution of each type of MFL is calculated using the finite-difference time-domain method. It is revealed that the hexagonal ring-type MFL has the best performance in power handling and maintaining beam quality. Further calculation indicates that power encircled in the diffraction-bucket of L-core MFL scales with no more than 0.4L, which chaJlenges the practical worthiness of fielding MFL with a large number of cores. 相似文献
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用于疾病诊断的Gd~Ⅲ/量子点多模态成像探针的构建 总被引:2,自引:0,他引:2
结合核磁共振成像(MRI)和荧光成像技术,以钆离子、近红外低毒量子点、二氧化硅和聚丙烯酸(PAA)等为原料,采用一系列纳米载体自组装技术,构建出MRI弛豫率/荧光效率高和生物相容性好的GdⅢ/量子点多模态纳米探针.结果表明,与未螯合GdⅢ的量子点纳米探针相比,GdⅢ/量子点多模态纳米探针具有更高的弛豫率;t1-加权MRI成像也证实了GdⅢ/量子点多模态纳米探针具有很好的阳性造影功效. 相似文献
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涉及两相正交各向异性体界面干涉问题的研究,多裂纹问题被分解为只含单裂纹的子问题,利用位错理论和裂面应力自由条件,列出一组可数值求解位错密度函数的奇异积分方程,从耐 注得应力强度因子。 相似文献
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The non-singular and bounded terms for stresses near the crack tip were investigated. The crack problem in a transversely isotropic piezoelectric solid for the plane problem was dealt with. The principle of superposition and the Plemelj formulation were introduced. The non-singular terms are given by solving Rieman-Hilbert problem. It is shown that the non-singular terms are influenced by the elastic and electric constants. 相似文献