排序方式: 共有29条查询结果,搜索用时 15 毫秒
1.
高效液相色谱法测定麻黄及其制剂中的麻黄类生物碱和川芎嗪 总被引:24,自引:0,他引:24
用RP HPLC分离测定了麻黄及其制剂中的麻黄类生物碱及川芎嗪。采用色谱柱Nova Pak C18(15 0mm×3.9mmi.d .) ,二极管阵列检测器 (DAD)。测定麻黄类生物碱时 ,以甲醇 0 .0 2mol/LKH2 PO4 乙酸 三乙胺 (体积比为 4∶96∶0 .2∶0 .0 1)为流动相 ,在 2 10nm波长下检测 ;测定川芎嗪时 ,以甲醇 水 乙酸 (体积比为 35∶6 5∶0 .5 )为流动相 ,在 2 90nm波长下检测。分别测定了麻黄原药材、中成药 (小儿清肺丸、鹭鸶咳丸 )中麻黄碱、伪麻黄碱、去甲基麻黄碱、去甲基伪麻黄碱和川芎嗪的含量。 相似文献
2.
3.
4.
5.
6.
Near-Field Fluorescence and Topography Characterization of a Single Nanometre Fluorophore by Apertureless Tip-Enhanced Scanning Near-Field Microscopy 下载免费PDF全文
Tip-enhanced near-field fluorescence and topography characterization of a single nanometre fluorophore is conducted by using an apertureless scanning near-field microscopy system. A fluorophore with size 80hm is mapped with a spatial resolution of 10hm. The corresponding near-field fluorescence data shows significant signal enhancement due to the apertureless tip-enhanced effect. With the nanometre spatial resolution capability and nanometre local tip-enhanced effect, the apertureless tip-enhanced scanning near-field microscopy may be further used to characterize a single molecule by realizing the local near-field spectrum assignment corresponding to topography at nanometre scale. 相似文献
7.
8.
9.
10.