离子束微探针及其扫描断层分析应用研究

以欧共体离子束物理及材料科学研究所的装置为例介绍了离子束微探针实验装置,给出了利用这一装置开展重离子弹性反冲核分析、研究氢在钛合金中的微观分布及其动力学行为的实验结果.该离子束微探针装置可以用来开展带电离子荧光分析、核反应分析、弹性反冲核分析、卢瑟福背散射分析及沟道效应和高离子束密度、大剂量离子注入等分析和研究工作.同时利用微束扫描分析可获得样品中元素的点、线、面分布信息.利用能量为16MeV、直径为3μm的Si5+离子束对钛合金中氢进行断层面扫描分析,观测到了氢在钛合金中的非均匀分布,揭示了氢在钛合金中的不同物理、化学状态与空间分布的相关性,为进一步研究钛的氢化和金属钛的表面腐蚀行为提供了科学依据. As an expmple, the nuclear micro-probe facility in the Forschungszentrum Rossendorf is introduced, which has a minimum beam size of 2 micrometers and can be used to perform particle induced X-ray emission (PIXE), nuclear reaction analysis (NRA), elastic recoil detection analysis (ERDA), Rutherford back scattering (RBS) and channeling etc. micro-beam analyses. By using single point, linear and lateral scanning, the elements composition and distribution in samples can be studied in micrometer scale...     

一台自制溅射负离子源的改进

自１９９５年以来，在中科院近物所２ＭＶ串列静电加速器上对溅射负离子源进行了调试．调试中对源体作了重大的改进，逐步完善了运行工艺，利用该离子源加速器可长时间提供Ｌｉ、Ｃ、Ｏ离子束.Since 1995, the sputter ion source has been tested on the 2 MV tandem acce lerator in the Institute of Modern Physics. During the experiment some important improvememts on the source were performed. The running procedure has been progressively perfect. With this vaurce, the stable Li, C,O ion beams can be delivered by the accelerator for long period.