排序方式: 共有6条查询结果,搜索用时 15 毫秒
1
1.
2.
基于在碱性条件下,银杏黄酮对CIO^--鲁米诺体系有显著的抑制作用,结合反相流动注射技术,建立了流动注射.抑制化学发光测定银杏提取物中的银杏黄酮。银杏黄酮质量浓度在0.4~14.0μg/ML范围与相对发光强度呈线性关系,检出限为0.06μg/ML,采样频率为120次/h,对10.0μg/ML的银杏黄酮平行测定11次,其RSD为1.2%,回收率为98、0%~104%。该方法可用于银杏黄酮制剂的测定。 相似文献
3.
4.
5.
A new Cu(Ⅰ) coordination polymer(CP) formulated as [Cu_2(L)(CN)_2]_n(1, L =1,1?-bis(5,6-dimethylbenzimidazole)methane) was synthesized, in which the cyanide anions were generated in situ by the cleavage of C–C bond of acetonitrile under hydrothermal conditions. CP 1 was characterized by elemental analysis, IR spectroscopy and single-crystal X-ray diffraction. It crystallizes in the orthorhombic system, Pccn space group, with a = 10.314(3), b = 20.966(7), c =9.432(3) ?, V = 2039.5(11) ?~3, Z = 4, C_(21) H_(20) Cu_2 N_6, M_r = 483.51, D_c = 1.575 g×cm~(-3), μ = 2.105 mm~(-1) and F(000) = 984, the final R = 0.0608 and wR = 0.1942 for 1226 observed reflections with Ⅰ 2s(Ⅰ)for the CP 1. The CP 1 possesses a 2D {63} layer structure which is composed of Cu(Ⅰ) centers bridged by L and CN– ligands. The thermal stability and luminescence properties of CP 1 are discussed in detail. The complex also displays a remarkable activity for the degradation of methyl orange by hydrogen peroxide in a Fenton-like process. 相似文献
1