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热重法测定碱性紫11:1的热稳定性及使用寿命 总被引:1,自引:0,他引:1
1 引言碱性紫11:1是一种广泛使用的染料,它应用于皮革、腈伦、革制品等染色.染色时,其使用寿命与操作温度密切相关,较高温度下使用,其寿命较短,乃至不宜使用.为了搞清上述关系,我们用TG法研究了碱性紫11:1的热稳定性及使用寿命. 相似文献
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We fabricate two Ni/Au-In0.17 Al0.83N/AlN/GaN Schottky diodes on substrates of sapphire and Si, respectively, and investigate their forward-bias current transport mechanisms by temperature-dependent current-voltage mea- surements. In the temperature range of 300-485K, the Schottky barrier heights (SBHs) calculated by using the conventional thermionic-emission (TE) model are strongly positively dependent on temperature, which is in contrast to the negative-temperature-dependent characteristic of traditional semiconductor Schottky diodes. By fitting the forward-bias I V characteristics using different current transport models, we find that the tunneling current model can describe generally the I V 5ehaviors in the entire measured range of temperature. Under the, high forward bias, the traditional TE mechanism also gives a good fit to the measured I-V data, and the actual barrier heights calculated according to the fitting TE curve are 1.434 and 1.413eV at 300K for InAlN/AlN/GaN Schottky diodes on Si and the sapphire substrate, respectively, and the barrier height shows a slightly negative temperature coefficient. In addition, a formula is given to estimate SBHs of Ni/Au-InAlN/AlN/GaN Schottky diodes taking the Fermi-level pinning effect into account. 相似文献
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本文对KBr压片法、KCl压片法以及萨特勒图谱采用的,糊剂法所绘制的三氯异氰尿酸的红外光谱进行了分析、对照。KCl压片法克服了溶剂的影响,简单、直观地体现了物质的精细结构。同时,将三氯异氰尿酸分别与KCl、KBr研磨,和三氯异氰尿酸纯品进行了紫外-可见吸收光谱对照。实验发现,与KBr研磨的三氯异氰尿酸和纯品的吸收峰有差异,而与KCl研磨后的三氯异氰尿酸和纯品一致,说明结构未发生变化。因此,认为KCl压片法是绘制三氯异氰尿酸红外光谱较好的方法。 相似文献
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