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本文首次提出采用升华物质为模板,制备聚苯胺包覆的中空硫电极材料.首先通过Na_2S_2O_3和稀HCl反应,在具有升华特性的ADD(2,4,6-三异丙基-1,3,5-三氧杂环己烷)微粒表面沉积一层S,然后在S的表面再沉积聚苯胺包覆层.在经60oC干燥12小时后,其中的ADD自然挥发,得到聚苯胺壳体包覆的中空硫复合物. SEM、TEM和TG分析表明,制得的聚苯胺包覆中空硫的粒径约为2μm,硫含量为61.1%.在500 m A·g~(-1)充放电电流下,首次放电比容量为776.2 m Ah·g~(-1),库仑效率为95.9%. 100次充放电循环后,放电比容量为524.7 m Ah·g~(-1).由于聚苯胺包覆物的聚苯胺膜具有抑制聚硫锂向外的扩散作用,以及包覆物中的空间对放电时S的膨胀具有缓冲作用,聚苯胺包覆中空硫粉末的放电比容量和充放电稳定性均明显高于未包覆聚苯胺的中空硫和化学制备的硫.这种制备导电聚合物包覆中空硫的新方法具有操作简单、成本低廉的优点,有进一步发展的前景.  相似文献   
2.
We study the phase coherence property of Bose-Einstein condensates confined in a one-dimensional optical lattice formed by a standing-wave laser field. The lattice depth is determined using a method of Kapitza-Dirac scattering between a condensate and a short pulse lattice potential. Condensates are then adiabatically loaded into the optical lattice. The phase coherence property of the confined condensates is reflected by the interference patterns of the expanded atomic cloud released from the optical lattice. For weak lattice, nearly all of the atoms stay in a superfluid state. However, as the lattice depth is increased, the phase coherence of the whole condensate sample is gradually lost, which confirms that the sub-condensates in each lattice well have evolved into number-squeezed states.  相似文献   
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通过直接的数值模拟,分析了原子束在激光驻波场下传播的动力学行为.估计了Cr原子沉积在基片上的焦点的大小,同时还发现一些实验参数会影响原子刻蚀的精度:如原子束的速度分布、激光的失谐量和激光束的直径等.  相似文献   
4.
大肠杆菌在细胞分裂时,FtsZ(Filamentous temperature-sensitive protein Z)蛋白会在细胞中部潜在位点聚合形成Z环,而MinC蛋白会抑制Z环形成,从而控制细胞分裂。本研究将min C与fts Z目的基因克隆到合适的载体中,并导入到大肠杆菌中进行表达,采用亲和层析和分子筛纯化的方法得到MinC/FtsZ复合物蛋白进行晶体筛选。通过FtsZ、MinC分别单独转化、表达纯化后混合和FtsZ、MinC共转化法两种方法得到FtsZ/MinC蛋白复合物,并分别对其进行晶体筛选。实验结果表明,在适宜的表达条件下,利用分别转化、纯化再混合的方法得到的FtsZ和MinC蛋白复合比例约为1∶1;混合时加入GTP和Mg Cl2可以促进复合物聚集态更单一,通过晶体筛选初步得到形状为针状的FtsZ/MinC复合蛋白晶体,为MinC/FtsZ复合物的结构解析提供实验基础。  相似文献   
5.
对甲氧基苯甲腈是一种重要的化学化工原料,本文采用超声分子束技术和共振多光子电离方法获得了对甲氧基苯甲腈的单色共振双光子电离光谱,基态S0到电子激发态S1的0←0跃迁被确定为(35549±2)cm~(-1),结合含时密度泛函理论计算结果对观察到的光谱进行了振动模式标识和描述.实验发现呼吸振动模非常易于激活,其基频和二次泛频光谱很强,三次泛频也可明确标识,观察到大量呼吸振动与其他正则模的结合振动,这是对甲氧基苯甲腈不同于常见的多原子分子的一个重要特性.这些结果为研究对甲氧基苯甲腈的里德堡态、动力学和零动能光谱等提供了重要的参考数据.  相似文献   
6.
We experimentally investigate the collective excitation of 87Rb Bose-Einstein condensates confined in a cigarshaped magnetic trap (QUIC trap). Using a method of magnetic perturbation, the center-of-mass oscillation of the condensate is excited, so that the radial trapping frequency of the QUIC trap can be precisely determined. A high-order excitation, characterized by a fast shape oscillation, also occurs simultaneously, with a noticeable damping in the oscillation amplitude compared with the oscillation of the center of mass. The measured oscillation frequencies, associated with these two low-energy excitation modes, agree well with theoretical predictions based on the Gross-Pitaevskii equation.  相似文献   
7.
We demonstrate a novel dual color magneto–optical trap (MOT), which uses two sets of overlapping laser beams to cool and trap 87 Rb atoms. The volume of cold cloud in the dual color MOT is strongly dependent on the frequency difference of the laser beams and can be significantly larger than that in the normal MOT with single frequency MOT beams. Our experiment shows that the dual color MOT has the same loading rate as the normal MOT, but much longer loading time, leading to threefold increase in the number of trapped atoms. This indicates that the larger number is caused by reduced light induced loss. The dual color MOT is very useful in experiments where both high vacuum level and large atom number are required, such as single chamber quantum memory and Bose–Einstein condensation (BEC) experiments. Compared to the popular dark spontaneous-force optical trap (dark SPOT) technique, our approach is technically simpler and more suitable to low power laser systems.  相似文献   
8.
We transfer cold ^87 Rb atoms from a vapour cell chamber to a spatially separated UHV magneto-optical trap (MOT) with the assistance of a red-detuned optical guiding beam and a normal push beam. Efficient optical guiding of the cold atoms is observed within a small detuning window. A pulsed optical guiding beam enhances the transfer efficiency and hence allows us to collect more atoms in UHV MOT in a shorter time, which is favourable for our experiment of achieving Bose-Einstein condensates (BEC). Besides the easy operation, another advantage of this optical guiding technique is also demonstrated such that slower atomic beams may be efficiently transferred along horizontal direction. This study is a direct application of the optical guiding technique as a powerful tool.  相似文献   
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