微型通风橱

简单介绍设计的微型通风橱在处理有毒气体上的应用，使有毒气体参与或产生的反应更环保。     

241Am-Be中子参考辐射的蒙特卡罗模拟研究

研究用于校准场所中子剂量监测仪表的241Am-Be中子参考辐射场计量特性。采用蒙特卡罗方法模拟了空气自由中子参考辐射(FRNR),GB/T 14055规定的最小尺寸中子参考辐射(SRNR)和实际中子参考辐射(ARNR)中不同检验点处中子周围剂量当量率、散射中子占比和能谱分布特征。研究结果表明,空气对FRNR中的剂量率和能谱分布影响小,近似为理想中子参考辐射;采用5%含硼聚乙烯作屏蔽的最小尺寸SRNR可减少热中子,降低散射中子占比,影锥法不适用于小尺寸中子参考辐射中对散射中子的修正;ARNR中的散射中子更少、占比更低,影锥法所得散射中子占比与理论值基本一致。     

Overview of finite elements simulation of temperature profile to estimate properties of materials 3D-printed by laser powder-bed fusion

Laser powder bed fusion(LPBF),like many other additive manufacturing techniques,offers flexibility in design expected to become a disruption to the manufacturing industry.The current cost of LPBF process does not favor a try-anderror way of research,which makes modelling and simulation a field of superior importance in that area of engineering.In this work,various methods used to overcome challenges in modeling at different levels of approximation of LPBF process are reviewed.Recent efforts made towards a reliable and computationally effective model to simulate LPBF process using finite element(FE)codes are presented.A combination of ray-tracing technique,the solution of the radiation transfer equation and absorption measurements has been used to establish an analytical equation,which gives a more accurate approximation of laser energy deposition in powder-substrate configuration.When this new analytical energy deposition model is used in in FE simulation,with other physics carefully set,it enables us to get reliable cooling curves and melt track morphology that agree well with experimental observations.The use of more computationally effective approximation,without explicit topological changes,allows to simulate wider geometries and longer scanning time leading to many applications in real engineering world.Different applications are herein presented including:prediction of printing quality through the simulated overlapping of consecutive melt tracks,simulation of LPBF of a mixture of materials and estimation of martensite inclusion in printed steel.     

用于细胞成像的双氰基二苯代乙烯衍生物双光子荧光银离子探针

双光子荧光显微成像兼具诸如近红外激发、暗场成像、避免荧光漂白和光致毒、定靶激发、高横向分辨率与纵向分辨率、降低生物组织吸光系数及降低组织自发荧光干扰等特点,显著地优于单光子荧光显微成像,为生命科学研究提供了更为便利的工具.因此双光子荧光探针适合于生物检测与成像.制备了衍生于二苯代乙烯的双光子荧光银离子探针,此探针以拥有异常大的双光子吸收截面(6TPA)的4-甲基-2,5-二氰基-4'-氨基二苯乙烯(DCS)作为双光子荧光母体,以6-芳基-3,9-二硫-6-氮杂癸烷(TAU)为Ag+配体.探针显示了大的δTPA(在MeCN中,950 GM)、对银离子有高的灵敏性与选择性、强的双光子荧光(790 nm激光激发时).探针的络合常数为IgK=5.76±0.05.探针能选择性地检测和成像活细胞中的游离Ag+,可用于细胞中微量Ag+的分析检测与成像.此探针为开发理想的双光子荧光探针提供了可供借鉴的平台.     

基于五氧化二钽集成非线性光波导的高重复频率 宽带平坦相干光频率梳的产生

通过波导结构设计以及色散调控,基于孤子脉冲压缩、自相位调制和光波分裂效应,用0.22 m反常色散五氧化二钽波导级联0.9 m正常色散五氧化二钽波导产生在1 520～1 580 nm波段具有4 dB平坦度、60 nm带宽的平坦光频率梳.利用X-Frog技术分析了脉冲在传输过程中的时谱演化,并且研究了产生光频率梳的相干性.时谱演化指出自相位调制和光波分裂的共同作用使得光频率梳的光谱包络变宽,并且具有良好的平坦度.一阶复互相干度计算指出光频率梳具有较好的相干性.仿真结果表明,五氧化二钽集成非线性光波导在产生高重复频率平坦相干宽带光频率梳方面具有较好的前景.     

原子核单粒子共振态的研究进展

共振是自然界普遍存在的有趣现象。在核物理领域，存在许多奇特现象，共振在其中扮演着重要角色。介绍了近期发展的RMF-CSM、RMF-CGF和RMF-CMR方法及其对原子核单粒子共振态的研究。给出了120Sn，31Ne等核的单粒子共振态的能量和宽度及其随质量数、形变的变化规律，分析了19C，31Ne和39Mg等核的晕形成的物理机制和在N=20附近能级反转的原因。特别是新发展的RMF-CMR方法，在描述稳定核和奇特核方面都取得了成功，支持Zr同位素存在巨晕的预言。Resonance is an interesting phenomenon in nature. In nuclear physics, resonance plays an important role in the formation of many exotic phenomena. This paper introduces the recently developed RMF-CSM, RMFCGF, and RMF-CMR methods and their researches on nuclear single-particle resonances. The energies and widths of the single-particle resonant states in 120Sn and 31Ne and their evolution to mass number and deformation are given. In addition, the physical mechanism of the halo formation in 19C, 31Ne and 39Mg and the cause of energy level inversion near N=20 are analyzed. In particular, the newly developed RMF-CMR approach has been successful in describing stable and exotic nuclei and supports the prediction that Zr isotopes exist in a giant halo.     

水平表面混合蒸气Marangoni凝结瞬态过程特性的实验研究

本文设计、搭建了水平表面上凝结换热实验系统,对水-酒精混合蒸气Marangoni凝结的瞬态过程进行了实验研究。研究发现:随着冷却水温度、酒精蒸气浓度的升高,在凝结瞬态过程中,表面过冷度先出现周期性变化,进而周期性减弱直至出现不规律变化。蒸气流速的升高总会促进表面过冷度出现周期性变化。结合实验过程中凝结形态变化规律,总结得到了凝结瞬态过程中的三种典型类型:成膜类型、液珠周期性运动类型与液珠不规律运动类型。     

基于三苯胺的双氰基二苯代乙烯型双光子荧光溶剂生色探针

以双氰基二苯代乙烯为双光子荧光母体,借助电子供体-π-电子受体(D-π-A)构-效关系,以二苯氨基作电子供体,氰基作电子受体,开发了一个新型的双光子荧光溶剂生色探针(SP1),并对其结构进行了表征.性能测试结果表明,SP1在环己烷和二甲亚砜(DMSO)中的最大发射波长分别为452和604 nm,显示出很宽的溶剂生色范围(152 nm),可用于溶剂极性与黏度的检测,亦能根据最大发射波长识别溶剂种类.SP1拥有较大的双光子吸收截面,在环己烷和DMSO中的最大双光子吸收截面分别为6670和2040 GM,并具有较大的斯托克斯位移(194 nm),其光稳定性、水溶性和细胞渗透性均比较优良.该探针可用于细胞中黏度的检测与成像.     

一种测试小分子迁移的新方法

针对高聚物材料中小分子的迁移现象,结合数字图像处理技术,提出了一种基于钠光和斐索等厚原理的光学干涉法.介绍了系统测试原理,针对光学系统的设计作了详细的分析与计算;通过实验测试,设计的光学系统能够采集到清晰的干涉条纹,且满足测试精度要求,由条纹间距随时间的变化测出了丙酮和乙醇小分子迁移时高聚物折射率的变化规律为:丙酮小分...     

Enhanced Photoluminescence of InGaN/GaN Green Light-Emitting Diodes Grown on Patterned Sapphire Substrate

Green InGaN/GaN based light-emitting diodes （LEDs） are fabricated both on planar and wet-etched patterned sapphire substrates by metalorganic vapour phase epitaxy （MOVPE）. Their photoluminescence （PL） properties of the two samples are studied. The results indicate that the PL integral intensity of the green LED on the patterned substrate is nearly two times of that on the planar one within the whole measured temperature range. The enhanced PL intensity in the green LED on the patterned substrate is shown completely contributed from the extraction efficiency, but not from the internal quantum efficiency. The conclusion is supported by temperature-dependent PL analysis on the two samples, and the mechanisms axe discussed.