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柳红军  周通  沈玉华  谢安建 《应用化学》2015,32(12):1410-1415
研究了Ce(Ⅲ)离子与巴比妥钠形成的配合物对双(对硝基苯基)磷酸酯(BNPP)的催化水解作用。 结果表明, Ce(Ⅲ)与巴比妥钠形成的配合物对BNPP的水解具有很高的催化活性,可使BNPP水解速率提高至自发水解时的1.52×108倍。 体系的pH值和温度对催化水解反应的影响,发现在温度为25 ℃和pH值为8.50的条件下,催化效果最佳。  相似文献   
2.
This paper reports that two identical external-cavity-diode-laser (ECDL) based spectrometers are constructed at 634 nm referencing on the hyperfine B-X transition R(80)8-4 of 127I2. The lasers are stabilized on the Doppler-free absorption signals using the third-harmonic detection technique. The instability of the stabilized laser is measured to be 2.8 × 10-12 (after 1000 s) by counting the beat note between the two lasers. The absolute optical frequency of the transition is, for the first time, determined to be 472851936189.5 kHz by using an optical frequency comb referenced on the microwave caesium atomic clock. The uncertainty of the measurement is less than 4.9 kHz.  相似文献   
3.
周通 《中学生数学》2012,(17):46-47
椭圆面积公式S=πab,其中π为圆周率,a、b分别是椭圆半短轴、半长轴的长.关于椭圆面积公式的证法有多种,文献[1]利用仿射变换与仿射不变量推导出椭圆面积公式,文献[2]通过对单位正方形的拉伸(压缩)变换前后面积关系的讨论,给出了椭圆面积公式的又一证法.文献[3]利用初等数学的方法,推导出椭圆面积的计算公式.本文利用投影和定积分知识相结合的方法,给出了任意曲边形面积公式,进而给出椭圆面积公式的一种新的证法.  相似文献   
4.
Coherent pulse stacking(CPS) is a new time-domain coherent addition technique that stacks several optical pulses into a single output pulse, enabling high pulse energy and high average power. A Z-domain model targeting the pulsed laser is assembled to describe the optical interference process. An algorithm, extracting the cavity phase and pulse phases from limited data, where only the pulse intensity is available, is developed to diagnose optical cavity resonators. We also implement the algorithm on the cascaded system of multiple optical cavities,achieving phase errors less than 1.0°(root mean square), which could ensure the stability of CPS.  相似文献   
5.
椭圆面积公式S=πab,其中π为圆周率,α、b分别是椭圆半短轴、半长轴的长.关于椭圆面积公式的证法有多种,文献[1]利用仿射变换与仿射不变量推导出椭圆面积公式,文献[2]通过对单位正方形的拉伸(压缩)变换前后面积关系的讨论,给出了椭圆面积公式的又一证法.文献[3]利用初等数学的方法,推导出椭圆面积的计算公式.本文利用投...  相似文献   
6.
An optical flequency comb phase-locked on an iodine frequency stabilized diode laser at 634 nm is constructed to transfer the accuracy and stability from the optical domain to the radio frequency domain. An external-cavity diode laser is frequency-stabilized on the Doppler-free absorption signals of the hyperfine transition R(80)8-4 using the third-harmonic detection technique. The instability of the ultra-stable optical oscillator is determined to be 7 ×10^-12 by a cesium atomic clock via the optical frequency comb's mass frequencv dividing technique.  相似文献   
7.
We construct an ultra-stable external-cavity diode laser via modulation transfer spectroscopy referencing on a hyperfine component of the ST Rb D2 lines at 780 nm. The Doppler-free dispersion-like modulation transfer signal is obtained with high signal-to-noise-ratio. The instability of the laser frequency is measured by beating with an optical frequency comb which is phase-locked to an ultra-stable oven controlled crystal oscillator. The Allan deviation is 3.9 × 10-13 at I s averaging time and 9.8 ×10-14 at 90s averaging time.  相似文献   
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