用分光光度法测定蜂胶超临界CO2萃取物中总黄酮含量

利用碱性条件下黄酮与Al3 生成粉红色络合物在可见光区510 nm处有最大吸收的特性,以芦丁为标样,采用分光光度法测定蜂胶超临界CO2萃取物中总黄酮含量,并与HPLC标准方法测定结果进行比较,发现各平行样的测定结果基本一致,最大偏差为268.38 mg/100 g,最小偏差为52.77 mg/100 g.该法简便快捷,结果相对准确,可作为蜂胶超临界CO2萃取物中总黄酮含量快速评估的一种方法.     

磷脂酰胆碱水溶液CMC的测定

磷脂酰胆碱水溶液ＣＭＣ的测定陈鲁生周武姜云生（山东师范大学化学系济南２５００１４）关键词磷脂酰胆碱临界胶束浓度磷脂酰胆碱是一种天然生物两性表面活性物质，也是一种重要的生命物质，具有广泛的用途［１］，由于磷脂酰胆碱的水溶性较差，所以较长时间以来对其溶液...     

具有随机扰动和多重变时滞的神经网络稳定性分析

考虑了一个具有多重时变时滞的随机神经网络的全局渐近稳定性问题.通过构造Lyapunov-Krasovskii函数并运用广义Ito公式,得到了一个充分条件,条件保证了神经网络在随机扰动下的全局均方渐近稳定性.最后通过一个数值实例验证了结果的有效性.     

二维原子晶体的低电压扫描透射电子显微学研究

二维原子晶体材料,如石墨烯和过渡金属硫族化合物等,具有不同于其块体的独特性能,有望在二维半导体器件中得到广泛应用.晶体中的结构缺陷对材料的物理化学性能有直接的影响,因此研究结构缺陷和局域物性之间的关联是当前二维原子晶体研究中的重要内容,需要高空间分辨率的结构研究手段.由于绝大部分二维原子晶体在高能量高剂量的电子束辐照下容易发生结构损伤,利用电子显微方法对二维原子晶体缺陷的研究面临诸多挑战.低电压球差校正扫描透射电子显微(STEM)技术的发展,一个主要目标就是希望在不损伤结构的前提下对二维原子晶体的本征结构缺陷进行研究.在STEM下,多种不同的信号能够被同步采集,包括原子序数衬度高分辨像和电子能量损失谱等,是表征二维原子晶体缺陷的有力工具,不但能对材料的本征结构进行单原子尺度的成像和能谱分析,还能记录材料结构的动态变化.通过调节电子束加速电压和电子辐照剂量,扫描透射电子显微镜也可以作为电子刻蚀二维原子晶体材料的平台,用于加工新型纳米结构以及探索新型二维原子晶体的原位制备.本综述主要以本课题组在石墨烯和二维过渡金属硫族化合物体系的研究为例,介绍低电压扫描透射电子显微学在二维原子晶体材料研究中的实际应用.     

High-resolution electron microscopy for heterogeneous catalysis research

Heterogeneous catalysts are the most important catalysts in industrial reactions. Nanocatalysts, with size ranging from hundreds of nanometers to the atomic scale, possess activities that are closely connected to their structural characteristics such as particle size, surface morphology, and three-dimensional topography. Recently, the development of advanced analytical transmission electron microscopy(TEM) techniques, especially quantitative high-angle annular darkfield(HAADF) imaging and high-energy resolution spectroscopy analysis in scanning transmission electron microscopy(STEM) at the atomic scale, strengthens the power of(S)TEM in analyzing the structural/chemical information of heterogeneous catalysts. Three-dimensional reconstruction from two-dimensional projected images and the real-time recording of structural evolution during catalytic reactions using in-situ(S)TEM methods further broaden the scope of(S)TEM observation. The atomic-scale structural information obtained from high-resolution(S)TEM has proven to be of significance for better understanding and designing of new catalysts with enhanced performance.     

Modified scaling function projective synchronization of chaotic systems

This paper investigates a kind of modified scaling function projective synchronization of uncertain chaotic systems using an adaptive controller. The given scaling function in the new method can be an equilibrium point, a periodic orbit, or even a chaotic attractor in the phase space. Based on LaSalle's invariance set principle, the adaptive control law is derived to make the states of two chaotic systems function projective synchronized. Some numerical examples are also given to show the effectiveness of the proposed method.     

Charge density wave states in phase-engineered monolayer VTe2

Charge density wave (CDW) strongly affects the electronic properties of two-dimensional (2D) materials and can be tuned by phase engineering. Among 2D transitional metal dichalcogenides (TMDs), VTe$_{2}$ was predicted to require small energy for its phase transition and shows unexpected CDW states in its T-phase. However, the CDW state of H-VTe$_{2}$ has been barely reported. Here, we investigate the CDW states in monolayer (ML) H-VTe$_{2}$, induced by phase-engineering from T-phase VTe$_{2}$. The phase transition between T- and H-VTe$_{2}$ is revealed with x-ray photoelectron spectroscopy (XPS) and scanning transmission electron microscopy (STEM) measurements. For H-VTe$_{2}$, scanning tunneling microscope (STM) and low-energy electron diffraction (LEED) results show a robust $2\sqrt 3 \times 2\sqrt 3 $ CDW superlattice with a transition temperature above 450 K. Our findings provide a promising way for manipulating the CDWs in 2D materials and show great potential in its application of nanoelectronics.     

一类动态系统可靠 D -稳定性条件 - LMI方法

考虑一类具有执行器和传感器故障的动力系统可靠鲁棒控制综合问题. 提出了一个系统 D -稳定的充分必要条件. 基于这一充分必要条件, 得到了可靠 H_∞ 控制器存在的条件. 接着用线性矩阵不等式(LMI)方法设计控制器, 使闭环系统当部分控制器件出现故障时鲁棒 D -稳定且具有H_∞性能. 最后通过一个仿真实例说明该文给出的方法及其有效性     

相关远域与不分明子集的超紧性

本文引入了α－相关远域族的概念，由此写义了一般不分明子集的超紧性。这种超紧性在人间的情形与「１」中的超紧性等价，在子集的情形以良肾性为特款，具有相应的关于良紧性的几乎所有性质。特别是基于这种超仿紧性的超紧性还是Ｌ－好的推广。