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1.
Aequationes mathematicae - For $$p\in (1,\infty )$$ , we establish several criteria of one-sided invertibility on spaces $$l^p=l^p(\mathbb {Z})$$ for discrete band-dominated operators being either...  相似文献   
2.
A novel and suitable energy-dispersive X-ray fluorescent (EDXRF) device, currently at the prototype stage, the Project OXIRIS (Orthovoltage X-Ray–Induced Radiation System), is presented for the simultaneous detection and treatment of cancer diseases. Monte Carlo simulation and experimental results of EDXRF signals from a small deep artificial tumor consisting of a solution of gold nanoparticles bio-targeted and immersed in a tissue-bioequivalent matrix are presented and compared. Briefly, the device consists of a dynamic orthovoltage X-ray fluence concentration coupled to confocal with an EDXRF system along with a sample holder for 3D scanning; all integrated and controlled by a dedicated software capable of controlling the whole operation functionalities: the X-ray source, the rotating arm, the sample holder, and the detection system. The software also includes dedicated subroutines for X-ray fluorescent spectra processing to correlate K-lines signal at each acquisition position with the corresponding high atomic number elements' concentration to produce a 3D distribution according to the user-defined grid. The confocal configuration ensures that the detected signal comes exclusively from the excited volume as defined by the bulk of the focal spot. Hence, the 3D image is achieved by scanning the sample holder through the movement of the sample-carrier stretcher moved by step motors in the 3 coordinated axes. The feasibility of the proposed methodology and the design of the prototype have been successfully demonstrated experimentally, targeting gold nanoparticles in water-equivalent phantoms.  相似文献   
3.
Journal of Solid State Electrochemistry - Rapid methods using batch injection analysis (BIA) with amperometric detection were developed for the determination of quercetin extracted from the...  相似文献   
4.
Electrodes modified by liquid films or plasticized polymeric membranes containing a redox species offer valuable alternatives for the study of ion transfers and bimolecular electron transfers at liquid–liquid interfaces with conventional electrode arrangements and stable interfaces. The ion-to-electron (or electron-to-electron) transducer affects the electrochemical signal, complicating the accurate analysis of experimental data. This can be reduced through the use of an electrode surface-attached redox species of well-defined electrochemical behaviour. As will be demonstrated, the voltammetry of these systems show significant deviations with respect to individual charge transfers, which must be considered for appropriate diagnosis and quantitative analysis. For this, a simple analytical theory is presented here, deducing mathematical expressions for the current–potential response, as well as for the potential difference at the two polarized interfaces, the surface excess of the redox species and the ion interfacial concentrations.  相似文献   
5.
A theoretical analysis on the electric double layer formed near the surface of an infinite cylinder with an elliptical cross section and a prescribed electric potential in an ionic conductor was performed using the linearized Gouy–Chapman theory. A semi-analytical solution in terms of the Mathieu functions was obtained. The distributions of the electric potential, cations, anions, and electric field were calculated. The effects of various physical and geometric parameters were examined. The fields vary rapidly near the elliptical boundary and are nearly uniform at far field. Electric field concentrations were found at the ends of the semi-major and semi-minor axes of the ellipse. These concentrations are sensitive to the physical and geometric parameters.  相似文献   
6.
This paper investigates quasi-periodic vibration-based energy harvesting in a delayed nonlinear MEMS device consisting of a delayed Mathieu–van der Pol–Duffing type oscillator coupled to a delayed piezoelectric coupling mechanism. We use the multiple scales method to approximate the quasi-periodic response and the related power output near the principal parametric resonance. The effect of time delay on the energy harvesting performance is studied. It is shown that for appropriate combination of time delay parameters, there exists an optimum range of excitation frequency beyond the resonance where quasi-periodic vibration-based energy harvesting is maximum. Numerical simulations are performed to confirm the analytical predictions.  相似文献   
7.
The present article is devoted to find some invariant solutions of the \((2+1)\)-dimensional Bogoyavlenskii equations using similarity transformations method. The system describes \((2+1)\)-dimensional interaction of a Riemann wave propagating along y-axis with a long wave along x-axis. All possible vector fields, commutative relations and symmetry reductions are obtained by using invariance property of Lie group. Meanwhile, the method reduces the number of independent variables by one, which leads to the reduction of Bogoyavlenskii equations into a system of ordinary differential equations. The system so obtained is solved under some parametric restrictions and provides invariant solutions. The derived solutions are much efficient to explain the several physical properties depending upon various existing arbitrary constants and functions. Moreover, some of them are more general than previously established results (Peng and Shen in Pramana 67:449–456, 2006; Malik et al. in Comput Math Appl 64:2850–2859, 2012; Zahran and Khater in Appl Math Model 40:1769–1775, 2016; Zayed and Al-Nowehy in Opt Quant Electron 49(359):1–23, 2017). In order to provide rich physical structures, the solutions are supplemented by numerical simulation, which yield some positons, negatons, kinks, wavefront, multisoliton and asymptotic nature.  相似文献   
8.
Metal halide perovskite nanomaterials emerged as attractive emitting materials for light-emitting diodes (LEDs) devices due to their high photoluminescence quantum yield (PLQY), narrow bandwidth, high charge-carrier mobility, bandgap tunability, and facile synthesis. In the past few years, it has been witnessed an unprecedented advance in the field of metal halide perovskite nanomaterials based LEDs (PeLEDs) with a rapid external quantum efficiency (EQE) increase from 0.1% to 14.36%. From the viewpoint of material chemistry, the chemical regulation of metal halide perovskite nanomaterials made a great contribution to the efficiency improvement of PeLEDs. In this review, we categorize the strategies of chemical regulation as A-site cation engineering, B-site ion doping, X-site ion exchange, dimensional confinement, ligand exchange, surface passivation and interface optimization of transport layers for improving the EQEs of PeLEDs. We also show the potentials of chemical regulation strategies to enhance the stability of PeLEDs. Finally, we present insight toward future research directions and an outlook to further improve EQEs and stabilities of PeLEDs aiming to practical applications.  相似文献   
9.
In the present study, a simple versatile extraction method based on supramolecular solvent microextraction followed by inductively coupled plasma atomic emission spectrometry was developed for the extraction, separation and determination of zirconium (Zr) from hafnium (Hf). Zr and Hf were complexed with bis(2,4,4-trimethylpentyl) phosphinic acid, to obtain hydrophobic complex, and extracted into supramolecular solvent phase. The effective parameters on the supramolecular solvent microextraction efficiency were studied and optimized by using two different optimization methods: one variable at a time and central composite design. Under the optimum conditions, the linear range of 0.3–200.0 and 2.0–200.0 µg L?1, detection limits (S/N = 3) of 0.1 and 0.6 µg L?1, and precisions (n = 5) of 3.2–4.9% and 3.0–5.1% were obtained for Zr and Hf, respectively. Finally, the proposed method has been successfully applied for the extraction and separation of these cations in zirconium ore sample.  相似文献   
10.
In this paper we study the limit cycles of some classes of piecewise smooth vector fields defined in the two dimensional torus. The piecewise smooth vector fields that we consider are composed by linear, Ricatti with constant coefficients and perturbations of these one, which are given in (3). Considering these piecewise smooth vector fields we characterize the global dynamics, studying the upper bound of number of limit cycles, the existence of non-trivial recurrence and a continuum of periodic orbits. We also present a family of piecewise smooth vector fields that posses a finite number of fold points and, for this family we prove that for any 2k number of limit cycles there exists a piecewise smooth vector fields in this family that presents k number of limit cycles and prove that some classes of piecewise smooth vector fields presents a non-trivial recurrence or a continuum of periodic orbits.  相似文献   
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